NAPHTHYLDIAZOMETHANE AS A DERIVATIZING AGENT FOR THE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY DETECTION OF BILE-ACIDS

被引：7

作者：

MATTHEES, DP ^{[1
]}

PURDY, WC ^{[1
]}

机构：

[1] MCGILL UNIV,DEPT CHEM,MONTREAL H3A 2K6,QUEBEC,CANADA

来源：

ANALYTICA CHIMICA ACTA | 1979年 / 109卷 / 01期

关键词：

D O I：

10.1016/S0003-2670(01)84240-9

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Bile acids are derivatized with 1-naphthyldiazomethane and separated by h.p.l.c. on silica gel columns with a hexane-tetrahydrofuran-methanol solvent. Reactions proceed quickly at room temperature under mild conditions, to give strongly absorbing species for u.v. detection. Deoxycholic acid can be detected in cat feces. © 1979.

引用

页码：161 / 164

页数：4

共 9 条

[1]

BLAU K, 1978, HDB DERIVATIVES CHRO, P49

[2]

CAREY JB, 1973, BILE ACIDS, V2, P68

[3]

ENEROTH P, 1969, LIPID CHROMATOGRAPHI, V2, P149

[4] NAPHTHYLDIAZOALKANES AS DERIVATIZING AGENTS FOR THE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETECTION OF FATTY-ACIDS [J].