SYNTHESIS, CRYSTAL-STRUCTURE AND CONFORMATION OF N2-DIBENZYL-N1-TRANS-BUTOXYCARBONYL HYDRAZINE

被引：0
|
作者：
GALDECKI, Z
LUCIAK, B
REDLINSKI, AS
KACZMAREK, K
LEPLAWY, MT
机构：
[1] TECH UNIV LODZ,INST ALLGEMEINE CHEM,PL-90924 LODZ,POLAND
[2] UNIV LODZ,INST PHYS,PL-90924 LODZ,POLAND
[3] TECH UNIV LODZ,INST ORGAN CHEM,PL-90924 LODZ,POLAND
来源：
MONATSHEFTE FUR CHEMIE | 1991年 / 122卷 / 1-2期
关键词：
N2-DIBENZYL-N1-TRANS-BUTOXYCARBONYL HYDRAZINE; CRYSTAL STRUCTURE; CONFORMATION;
D O I：
10.1007/BF00815162
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The synthesis and the crystal structure of N2-dibenzyl-N1-butoxycarbonyl hydrazine are reported. The compound was prepared from commercially available t-butyl carbazate. It crystallizes in the triclinic space group P 1 with a = 5.479(1) angstrom, b = 9.559(1) angstrom, c = 9.748(1) angstrom, alpha = 63.81(1)-degrees, beta = 87.52(1)-degrees, gamma = 74.07(1) angstrom, Z = 1, D = 1.18 g/cm3. The structure was solved by direct methods and refined to R = 0.0329.
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收藏
页码：37 / 42
页数：6
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