Volatile, fatty acid, and triacylglycerol components of crude Egyptian mandarine peel oil were determined by dynamic headspace capillary gas chromatography mass spectrometric analysis, capillary gas chromatography, and reversed-phase high performance liquid chromatography with flame ionization detection, respectively. Mandarine peel oil contained 1.8% crude oil, of which 0.6% was triacylglycerol with respect to peel weight. Dipalmitoyllinoleoyl was the most abundant triacylglycerol present at 22.0%. Mandarine peel is currently a waste product of the Egyptian citrus industry. The fatty acid composition of the triacylglycerol oil was 19.6% palmitic, 2.8% stearic, 12.0% oleic, 55.4% linoleic, and 8.9% linolenic. The volatile portion of crude mandarine peel oil contained four major components in concentration 10% or greater: 37.4% limonene, 20.0% gamma-terpinolene, 15.2% beta-myrcene and 9.5% delta-3-carene.