SYNTHESIS AND NMR SPECTROSCOPIC INVESTIGATION OF A MACROCYCLIC DIPHOSPHINE LIGAND AND ITS NICKEL(II) AND PALLADIUM(II) COMPLEXES

被引：15

作者：

WIDHALM, M

KALCHHAUSER, H

KAHLIG, H

机构：

[1] Institut für Organische Chemie, Universität Wien, Wien, A-1090

来源：

HELVETICA CHIMICA ACTA | 1994年 / 77卷 / 01期

关键词：

D O I：

10.1002/hlca.19940770138

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The preparation of a macrocyclic diphosphine ligand 5 incorporating a binaphthyl unit and its Ni-II and Pd-II complexes, 6 and 7, is described. A complete assignment of H-1,- C-13-, and P-31-NMR data on the basis of 2D NMR spectroscopy (H-1, H-1-, C-13, H-1-, P-31, H-1-, P-31, C-13-COSY) was possible for 5, and also - in part - for 6 and 7.

引用

页码：409 / 418

页数：10

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