Three new phenylethanoid glycosides, 2-(4-hydroxyphenyl)ethyl-beta-D-apiosyl-(1 --> 6)-beta-D-glucopyranoside (osmanthuside H), 2-(4-hydroxyphenyl)ethyl 5-O-trans-p-coumaroyl-beta-D-apiosyl-(1 --> 6)-beta-D-glucopyranoside (osmanthuside I) and 244-hydroxyphenyl)ethyl 5-O-trans-feruloyl-beta-D-apiosyl-(1 --> 6)-beta-D-glucopyranoside (osmanthuside J), were isolated from the bark of Osmanthus asiaticus. The structures were elucidated on the basis of spectroscopic evidence.