2-((1E)-1-{2-[(2Z)-3,4-Diphenyl-2,3-di-hydro-1,3-thiazol-2-ylidene]hydrazin-1-ylidene}ethyl)pyridin-1-ium-bromide monohydrate

被引：4
|
作者：
Akkurt, Mehmet [1 ]
Mague, Joel T. [2 ]
Mohamed, Shaaban K. [3 ,4 ]
Hassan, Alaa A. [4 ]
Albayati, Mustafa R. [5 ]
机构：
[1] Erciyes Univ, Dept Phys, Fac Sci, TR-38039 Kayseri, Turkey
[2] Tulane Univ, Dept Chem, New Orleans, LA 70118 USA
[3] Manchester Metropolitan Univ, Chem & Environm Div, Manchester M1 5GD, Lancs, England
[4] Menia Univ, Chem Dept, Fac Sci, El Minia 61519, Egypt
[5] Kirkuk Univ, Dept Chem, Coll Sci, Kirkuk, Iraq
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷
关键词：
single-crystal X-ray study; T=150 K; mean sigma(C-C) = 0.004 A(degrees); R factor = 0.027; wR factor = 0.060; data-to-parameter ratio = 20.5;
D O I：
10.1107/S1600536814006229
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C22H19N4S +·Br-·H2O, the dihedral angles between the phenyl groups and the mean plane of the thiazolylidene ring are 34.69(13) and 64.27(13)°, respectively, while that between the thiazolylidene and pyridinium rings is 14.73(13)°. In the crystal, zigzag chains of alternating bromide ions and water molecules associate through O-H..Br interactions run in channels approximately parallel to the b axis. These chains help form parallel chains of cations through N-H..O, C-H..N and C-H..Br hydrogen bonds.
引用
收藏
页码：O478 / +
页数：9
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