2-((1E)-1-{2-[(2Z)-3,4-Diphenyl-2,3-di-hydro-1,3-thiazol-2-ylidene]hydrazin-1-ylidene}ethyl)pyridin-1-ium-bromide monohydrate

被引：4
|
作者：
Akkurt, Mehmet [1 ]
Mague, Joel T. [2 ]
Mohamed, Shaaban K. [3 ,4 ]
Hassan, Alaa A. [4 ]
Albayati, Mustafa R. [5 ]
机构：
[1] Erciyes Univ, Dept Phys, Fac Sci, TR-38039 Kayseri, Turkey
[2] Tulane Univ, Dept Chem, New Orleans, LA 70118 USA
[3] Manchester Metropolitan Univ, Chem & Environm Div, Manchester M1 5GD, Lancs, England
[4] Menia Univ, Chem Dept, Fac Sci, El Minia 61519, Egypt
[5] Kirkuk Univ, Dept Chem, Coll Sci, Kirkuk, Iraq
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷
关键词：
single-crystal X-ray study; T=150 K; mean sigma(C-C) = 0.004 A(degrees); R factor = 0.027; wR factor = 0.060; data-to-parameter ratio = 20.5;
D O I：
10.1107/S1600536814006229
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C22H19N4S +·Br-·H2O, the dihedral angles between the phenyl groups and the mean plane of the thiazolylidene ring are 34.69(13) and 64.27(13)°, respectively, while that between the thiazolylidene and pyridinium rings is 14.73(13)°. In the crystal, zigzag chains of alternating bromide ions and water molecules associate through O-H..Br interactions run in channels approximately parallel to the b axis. These chains help form parallel chains of cations through N-H..O, C-H..N and C-H..Br hydrogen bonds.
引用
收藏
页码：O478 / +
页数：9
相关论文
共 50 条
  • [1] 2-((1E)-1-{2-[(2Z)-4-(4-Bromophenyl)3-phenyl-2,3-dihydro-1,3-thiazol-2-ylidene]hydrazin-1-ylidene}ethyl)pyridin1-ium bromidemonohydrate
    Mague, Joel T.
    Mohamed, Shaaban K.
    Akkurt, Mehmet
    El-Alaziz, Ahmed T. Abd
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O328 - +
  • [2] Crystal structure of 4-((1E)-1-{(2Z)-2-[ 4(4-bromophenyl)-3-phenyl-2,3-dihydro1,3-thiazol-2-ylidene] hydrazin-1-ylidene}ethyl)phenol hemihydrate
    Mague, Joel T.
    Akkurt, Mehmet
    Mohamed, Shaaban K.
    Hassan, Alaa A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O1124 - +
  • [3] n-Butyldichlorido(2-{(1E)-1-[2-(pyridin-2-yl)hydrazin-1-ylidene]ethyl}phenolato)tin(IV)
    Abu Affan, Md.
    Chee, Dayang N. A.
    Ahmad, Fasihuddin B.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M1412 - U707
  • [4] (Z)-1-[(2E)-3,4-Diphenyl-2,3-dihydro1,3-thiazol-2-ylidene]-2-[1-(4-hydroxyphenyl)ethylidene]hydrazinium bromide including an unknown solvate
    Mague, Joel T.
    Mohamed, Shaaban K.
    Akkurt, Mehmet
    Hassan, Alaa A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O647 - +
  • [5] Methyl 2-((2Z, 5Z)-4-oxo-3-phenyl-2-{2-[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]hydrazin-1-ylidene}-1,3-thiazolidin-5-ylidene)acetate
    Mague, Joel T.
    Akkurt, Mehmet
    Mohamed, Shaaban K.
    Hassan, Alaa A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O436 - +
  • [6] (1Z, 2E)-1-( 3,4-Diphenyl-2,3-dihydro-1,3thiazol-2-ylidene)-2-(1-p-tolylethylidene)hydrazine
    Mohamed, Shaaban K.
    Mague, Joel T.
    Akkurt, Mehmet
    Hassan, Alaa A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1324 - +
  • [7] Crystal structure of ethyl 2-(2-{(1E)-[(E)-2-(2-hydroxybenzylidene)hydrazin-1-ylidene]methyl}phenoxy)acetate
    Akkurt, Mehmet
    Mague, Joel T.
    Mohamed, Shaaban K.
    Ahmed, Eman A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O70 - U267
  • [8] 2-{(E)-1-[2-(4-Nitrophenyl) hydrazin-1-ylidene] ethyl}benzene-1,3-diol
    Howie, R. Alan
    Wardell, James L.
    Wardell, Solange M. S. V.
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O685 - U1962
  • [9] Crystal structure of (E)-1-(3-benzyl-5-phenyl-1,3-thiazol-2-ylidene)-2-[(E)-1,2,3,4-tetrahydronaphthalen-1-yliciene]hydrazin-1-ium bromide
    Mohamed, Shaaban K.
    Elgarhy, Sahar M., I
    Hassan, Alaa A.
    Demirtas, Gunes
    Mague, Joel T.
    Ramli, Youssef
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2021, 77 : 420 - +
  • [10] Crystal structure of ethyl 2-[2-((1E)-{(1E)-2-[2-(2-ethoxy-2-oxoethoxy)benzylidene]hydrazin-1-ylidene}methyl)phenoxy]acetate
    Mague, Joel T.
    Mohamed, Shaaban K.
    Akkurt, Mehmet
    Ahmed, Eman A.
    Omran, Omran A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O16 - +
12345