LABORATORY-SCALE SETUP FOR ANIONIC-POLYMERIZATION UNDER INERT ATMOSPHERE

被引：165

作者：

NDONI, S

PAPADAKIS, CM

BATES, FS

ALMDAL, K

机构：

[1] RISO NATL LAB,DEPT SOLID STATE PHYS,DK-4000 ROSKILDE,DENMARK

[2] UNIV COPENHAGEN,DEPT CHEM,DK-2100 COPENHAGEN,DENMARK

[3] ROSKILDE UNIV CTR,DEPT STUDIES MATH & PHYS & FUNCT EDUC RES & APPLI,DK-4000 ROSKILDE,DENMARK

[4] DEPT CHEM ENGN & MAT SCI,MINNEAPOLIS,MN 55405

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 1995年 / 66卷 / 02期

关键词：

D O I：

10.1063/1.1146052

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

''Living'' anionic polymerization offers a readily feasible preparation of very well-controlled homo- or copolymers in a wide range of molar masses and chemical structures. Such samples are vital in experimental polymer physics and the technique presented here offers self-sufficiency with such samples. The technique of anionic polymerization performed under inert atmosphere is presented here. The components of the setup are described in detail. Purification procedures for glassware and chemicals for specific polymerizations are given. Illustrative examples and results are presented. © 1995 American Institute of Physics.

引用

页码：1090 / 1095

页数：6

共 18 条

[1] PREPARATION OF HIGH-PURITY, ANIONIC-POLYMERIZATION GRADE ALKYL METHACRYLATE MONOMERS [J].