CHARACTERIZATION OF TIB2-TI(CN)-NI CERAMICS BY TRANSMISSION AND ANALYTICAL ELECTRON-MICROSCOPY

被引:6
|
作者
DAI, JY [1 ]
LI, DX [1 ]
YE, HQ [1 ]
ZHANG, GJ [1 ]
JIN, ZZ [1 ]
机构
[1] CHINA BLDG MAT ACAD,INST ADV CERAM,BEIJING 100024,PEOPLES R CHINA
基金
中国国家自然科学基金;
关键词
Hot pressing - Microscopic examination - Microstructure - Nickel - Phase transitions - Titanium compounds - Transmission electron microscopy;
D O I
10.1016/0167-577X(93)90200-H
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The microstructure of TiB2-Ti (CN)-Ni ceramics has been investigated by means of transmission and analytical electron microscopy. In many cases, TiB2 and Ti(CN) grew together with a unique orientation relationship. However, Ti(CN) particles were also found to precipitate in TiB2 crystals, and a different orientation relationship between precipitated Ti (CN) particles and TiB2 crystals can be detected. The TiB2/Ti(CN) interface was investigated using high-resolution electron microscopy. During hot-press procession, two Ni-rich intergranular phases with N31Si12 and N16Ti6Si7 type structures and amorphous phase were formed on grain boundaries.
引用
收藏
页码:317 / 321
页数:5
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