FORENSIC ANALYSIS OF EXPLOSIVES USING ION-CHROMATOGRAPHIC METHODS

被引:60
作者
MCCORD, BR
HARGADON, KA
HALL, KE
BURMEISTER, SG
机构
[1] FBI LAB,MAT ANAL UNIT,WASHINGTON,DC 20535
[2] LAFAYETTE COLL,NEWARK,DE 19713
关键词
ELECTROPHORESIS; ION CHROMATOGRAPHY; EXPLOSIVES; FORENSIC ANALYSIS;
D O I
10.1016/0003-2670(94)85115-8
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Applications of ion chromatographic analysis techniques including capillary electrophoresis and inverse photometric detection are explored in the analysis of low explosives and their residues. Past procedures for this analysis are reviewed and new techniques are introduced. A scheme for the investigation of trace evidence from bombing crime scenes using ion chromatographic techniques is developed. This scheme includes two sets of anionic and cationic analytical methods to allow identification and confirmation of the presence of inorganic explosive residue. Several different types of explosive devices are examined using this scheme, and the results are shown.
引用
收藏
页码:43 / 56
页数:14
相关论文
共 30 条
[1]  
BARSOTTI DJ, 1983, P INT S AN DET EXPL, P209
[2]  
BENDER EC, 1989, CRIME LAB DIGEST, V16, P78
[3]  
BEVERIDGE A, 1986, J ENERG MATER, V4, P29
[4]  
Beveridge A D, 1975, J Forensic Sci, V20, P431
[5]  
BUECHELE RC, 1982, ANAL CHEM, V54, P502
[6]  
CONKLING JA, 1985, CHEM PYROTECHNICS, P136
[7]   CAPILLARY ZONE ELECTROPHORESIS OF RARE-EARTH-METALS WITH INDIRECT UV ABSORBENCY DETECTION [J].
FORET, F ;
FANALI, S ;
NARDI, A ;
BOCEK, P .
ELECTROPHORESIS, 1990, 11 (09) :780-783
[8]   FACTORS AFFECTING THE RESOLUTION AND DETECTABILITY OF INORGANIC ANIONS BY NON-SUPPRESSED ION CHROMATOGRAPHY [J].
GLATZ, JA ;
GIRARD, JE .
JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1982, 20 (06) :266-273
[9]   INDIRECT FLUORIMETRIC DETECTION AND QUANTIFICATION IN CAPILLARY ZONE ELECTROPHORESIS OF INORGANIC ANIONS AND NUCLEOTIDES [J].
GROSS, L ;
YEUNG, ES .
JOURNAL OF CHROMATOGRAPHY, 1989, 480 :169-178
[10]  
HANDERSON IK, 1991, OCT P INT S ION CHRO, P30