DETERMINATION OF BIOGENIC-AMINES AND OTHER AMINES IN WINE BY AN OPTIMIZED HPLC METHOD WITH POLARITY GRADIENT ELUTION

被引：0
作者：
CRESPO, MI
LASA, BV
机构：
来源：
AMERICAN JOURNAL OF ENOLOGY AND VITICULTURE | 1994年 / 45卷 / 04期
关键词：
AMINES; WINE; OPTIMIZATION POLARITY GRADIENT;
D O I：
暂无
中图分类号：
Q81 [生物工程学（生物技术）]; Q93 [微生物学];
学科分类号：
071005 ; 0836 ; 090102 ; 100705 ;
摘要：
An optimized method to determine biogenic amines and other amines in wine with pre-column derivatization with o-phthaldialdehyde is reported. Determination of the different amines has been carried out using a polarity gradient elution technique involving methanol and sodium acetate buffer. The method has been optimized in terms of its precision and accuracy assessed by statistical means using formula derived for the purpose of treating determined number sets of data. After validation, the method was applied to determine amines in red, white, and rose wines of Rioja region.
引用
收藏
页码：460 / 463
页数：4
相关论文
共 17 条
[1]  
BATTAGLIA R, 1978, J HIGH RES CHROMATOG, V2, P100
[2]  
Bravo F., 1986, Alimentaria, P65
[3]  
HORWITZ W, 1980, J ASSOC OFF ANA CHEM, V63, P1344
[4]  
LAFONLAFOURCADE S, 1975, VIGNE VIN, V2, P103
[5]  
LARRAINA G, 1993, CHARACTERIZACION ANA
[6]   AMINES IN FOODS [J].
MAGA, JA .
CRC CRITICAL REVIEWS IN FOOD SCIENCE AND NUTRITION, 1978, 10 (04) :373-403
[7]  
MARCE RM, 1989, AM J ENOL VITICULT, V40, P194
[8]  
OUGH CS, 1981, AM J ENOL VITICULT, V32, P185
[9]  
PFEIFFER P, 1992, AM J ENOL VITICULT, V43, P315
[10]  
RENON P, 1979, IND ALIMENT MAGGIO, P365
12