DETECTION AND IDENTIFICATION OF ANABOLIC-STEROIDS IN BOVINE URINE BY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY

被引：39
作者：
LEBIZEC, B
MONTRADE, MP
MONTEAU, F
ANDRE, F
机构：
[1] ENVN (Ministère de l'Agriculture), Laboratoire des Dosages Hormonaux, 44087 Nantes Cedex 03
来源：
ANALYTICA CHIMICA ACTA | 1993年 / 275卷 / 1-2期
关键词：
GAS CHROMATOGRAPHY MASS SPECTROMETRY; ANABOLIC STEROIDS; BOVINE URINE; HORMONES; URINE;
D O I：
10.1016/0003-2670(93)80283-Q
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Within the scope of the national plan for hormone control in France, a study was made to develop a system for the control of the illegal use of anabolic steroids for fattening purposes in animal production. A screening procedure for these residues in bovine urine was developed, based on C18 solid-phase extraction, silica gel purification and gas chromatographic-mass spectrometric analysis with selected ion monitoring. All the method parameters are discussed, especially the enzymatic and chemical hydrolysis steps and the choice of derivatives.
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页码：123 / 133
页数：11
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