1-(3,4-Difluorobenzyl)-4-(4-methyl-phenylsulfonyl)piperazine

被引:0
作者
Sreenivasa, S. [1 ]
Anitha, H. C. [2 ,3 ]
Suchetan, P. A. [2 ,3 ]
Palakshamurthy, B. S. [4 ]
Savanur, J. [5 ]
Tonannavar, J. [5 ]
机构
[1] Tumkur Univ, Dept Studies & Res Chem, Tumkur 572103, Karnataka, India
[2] Tumkur Univ, Ctr Adv Mat, Tumkur 572103, Karnataka, India
[3] Tumkur Univ, Dept Chem, Tumkur 572103, Karnataka, India
[4] Tumkur Univ, Dept Studies & Res Phys, UCS, Tumkur 572103, Karnataka, India
[5] Karnatak Univ, Dept Phys, Dharwad 580003, Karnataka, India
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷
关键词
D O I
10.1107/S1600536813016462
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C18H20F2N2O2S, the central piperazine ring adopts a chair conformation. The dihedral angle between the two benzene rings is 40.20 degrees, whereas those between the piperazine ring (considering the best fit plane through all the non-H atoms) and the sulfonyl-bound benzene and difluorobenzene rings are 74.96 and 86.16 degrees, respectively. In the crystal, molecules are stacked along the a axis through weak CH center dot center dot center dot O and C-H center dot center dot center dot F interactions.
引用
收藏
页码:O1179 / +
页数:8
相关论文
共 6 条
  • [1] Bruker, 2009, APEX2 SADABS SAINT P
  • [2] Mercury CSD 2.0 -: new features for the visualization and investigation of crystal structures
    Macrae, Clare F.
    Bruno, Ian J.
    Chisholm, James A.
    Edgington, Paul R.
    McCabe, Patrick
    Pidcock, Elna
    Rodriguez-Monge, Lucia
    Taylor, Robin
    van de Streek, Jacco
    Wood, Peter A.
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2008, 41 : 466 - 470
  • [3] A short history of SHELX
    Sheldrick, George M.
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
  • [4] An unknown solvate of 1-(2,4-dichlorobenzyl)-4-[(4-methylphenyl)sulfonyl]piperazine
    Sreenivasa, S.
    ManojKumar, K. E.
    Anitha, H. C.
    Suchetan, P. A.
    Palakshamurthy, B. S.
    Jayashree, Yenagi
    Tonannavar, J.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O782 - +
  • [5] 1-Tosyl-4-[2-(trifluoromethyl)benzyl]-piperazine
    Sreenivasa, S.
    Anitha, H. C.
    ManojKumar, K. E.
    Tonannavar, J.
    Jayashree, Yenagi
    Suchetan, P. A.
    Palakshamurthy, B. S.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O239 - +
  • [6] (2,3-Difluorophenyl)(4-tosylpiperazin-1yl)methanone
    Sreenivasa, S.
    ManojKumar, K. E.
    Suchetan, P. A.
    Tonannavar, J.
    Chavan, Yashshwita
    Palakshamurthy, B. S.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O185 - +