SYNTHESIS OF 2,3,4,5-TETRANITROPYRROLE

被引：20

作者：

HINSHAW, JC ^{[1
]}

EDWARDS, WW ^{[1
]}

GEORGE, C ^{[1
]}

GILARDI, R ^{[1
]}

机构：

[1] USN,RES LAB,STRUCT MATTER LAB,WASHINGTON,DC 20375

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 1992年 / 29卷 / 07期

关键词：

D O I：

10.1002/jhet.5570290708

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Dealkylation of 1-tert-butyl-2,3,4-trinitropyrrole in boiling trifluroacetic acid gave 2,3,4-trinitropyrrole, the structure of which was confirmed by X-ray crystallography. Treatment of this trinitropyrrole with nitric acid/oleum briefly at 60-degrees gave 2,3,4,5-tetranitropyrrole.

引用

页码：1721 / 1724

页数：4

共 10 条

[1]

[Anonymous], 1974, INT TABLES XRAY CRYS, VIV

[2] SYNTHESIS OF POLYNITROBENZENES - OXIDATION OF POLYNITROANILINES AND THEIR N-HYDROXY, N-METHOXY, AND N-ACETYL DERIVATIVES [J].