CRYSTAL-STRUCTURE OF LIGNOCAINE HYDROCHLORIDE - NICKEL THIOCYANATE COMPLEX

被引：2
|
作者：
INDIRA, A
SRIDHAR, MA
PRASAD, JS
CAMERON, TS
机构：
[1] UNIV MYSORE,DEPT STUDIES PHYS,MYSORE 570006,KARNATAKA,INDIA
[2] DEPT CHEM,HALIFAX,NS,CANADA
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE | 1994年 / 209卷 / 05期
关键词：
CHARGE-TRANSFER COMPLEX;
D O I：
10.1524/zkri.1994.209.5.440
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, Ni0.5S2C16H24O2N4, crystallizes in the monoclinic space group P2(1)/a with a = 15.062(3) angstrom, b = 7.829(2) angstrom, c = 18.527(2) angstrom, beta = 110.179(9)degrees, Z = 4. The structure was solved by SHELXS-86 using 1772 out of 4524 reflections with I > 3sigma(I). Full-matrix refinement gave a final residual of R(f) = 0.0573. The nickel is in a distorted octahedral coordination and it does not show any hydrogen bonding. The packing of the molecules shows a layered arrangement down b.
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页码：440 / 442
页数：3
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