CHARACTERIZATION OF POLYAMIDE-6 MADE BY REACTIVE EXTRUSION .2. ANALYSIS OF MICROSTRUCTURE

被引：12
作者：
HORNSBY, PR
TUNG, JF
机构：
[1] Department of Materials Technology, Brunel University, Uxbridge, Middlesex
来源：
JOURNAL OF APPLIED POLYMER SCIENCE | 1994年 / 54卷 / 07期
关键词：
D O I：
10.1002/app.1994.070540709
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Consideration is given to the characterization of microstructure in polyamide 6 prepared by polymerization of epsilon-caprolactam in a corotating twin-screw extruder. Results obtained by FTIR, WAXD, DSC, and DMTA are discussed in terms of the molecular mass of the polymer, the thermal history of the material, and the influence of residual monomer. (C) 1994 John Wiley and Sons, Inc.
引用
收藏
页码：899 / 907
页数：9
相关论文
共 20 条
[1]   ALPHA-GAMMA TRANSITION OF NYLON 6 [J].
ARIMOTO, H .
JOURNAL OF POLYMER SCIENCE PART A-GENERAL PAPERS, 1964, 2 (5PA) :2283-&
[2]   EFFECT OF POLYMERIZATION CONDITIONS AND CRYSTALLINITY ON MECHANICAL-PROPERTIES AND FRACTURE OF SPHERULITIC NYLON-6 [J].
BESSELL, TJ ;
HULL, D ;
SHORTALL, JB .
JOURNAL OF MATERIALS SCIENCE, 1975, 10 (07) :1127-1136
[3]  
BRILL R, 1942, PHYS CHEM B, V53, P61
[4]   CHANGES IN THE MORPHOLOGY OF BULK SPHERULITIC NYLON-6 DUE TO PLASTIC-DEFORMATION [J].
GALESKI, A ;
ARGON, AS ;
COHEN, RE .
MACROMOLECULES, 1988, 21 (09) :2761-2770
[5]  
GALESKI A, 1987, MAKROMOL CHEM, V188, P1195
[6]   RELATIONSHIPS BETWEEN MECHANICAL PROPERTIES AND RELAXATION PROCESSES IN POLMER - NYLON 6 [J].
GARBUGLIO, C ;
AJROLDI, G ;
CASIRAGHI, T ;
VITTADINI, G .
JOURNAL OF APPLIED POLYMER SCIENCE, 1971, 15 (10) :2487-+
[7]   THE CRYSTAL STRUCTURE OF POLYCAPROAMIDE - NYLON-6 [J].
HOLMES, DR ;
BUNN, CW ;
SMITH, DJ .
JOURNAL OF POLYMER SCIENCE, 1955, 17 (83) :159-177
[8]  
HORNSBY PR, IN PRESS J APPL POLY
[9]  
ILLERS KH, 1972, MAKROMOLEKUL CHEM, V158, P285
[10]  
ISMAT A, 1971, J POLYM SCI POL CHEM, V9, P199
12