HIGH-PRESSURE LIQUID-CHROMATOGRAPHIC METHOD FOR THE DETERMINATION OF CARBOFURAN RESIDUES IN SOIL AND WATER

被引:20
作者
NELSEN, TR [1 ]
COOK, RF [1 ]
机构
[1] FMC CORP,DEPT RES & DEV,AGR CHEM GRP,MIDDLEPORT,NY 14105
关键词
D O I
10.1021/jf60226a026
中图分类号
S [农业科学];
学科分类号
09 ;
摘要
A method for residue analysis of carbofuran (2, 3-dihydro-2, 2-dimethyl-7-benzofuranyl methylcarbamate) capable of quantitation of residues at the 0.10 ppm level in soil and water is presented. The method involves a methanol/water extraction, base hydrolysis of carbofuran to its phenolic moiety, and quantitation of the phenol which was accomplished by high-pressure liquid chromatography using a UV absorbance detector at 280 nm. Method recovery averaged 82.4 ± 8.3% for soil and 82.2 ± 9.6% for water. © 1979, American Chemical Society. All rights reserved.
引用
收藏
页码:1186 / 1188
页数:3
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