DETERMINATION OF ETHANOLAMINE IN WINE BY HPLC AFTER DERIVATIZATION WITH 9-FLUORENYLMETHOXYCARBONYLCHLORIDE

被引：0

作者：

PFEIFFER, P

RADLER, F

机构：

来源：

AMERICAN JOURNAL OF ENOLOGY AND VITICULTURE | 1992年 / 43卷 / 04期

关键词：

ETHANOLAMINE; HPLC;

D O I：

暂无

中图分类号：

Q81 [生物工程学（生物技术）]; Q93 [微生物学];

学科分类号：

071005 ; 0836 ; 090102 ; 100705 ;

摘要：

A method was developed for the determination of ethanolamine in grape must and wine. Ethanolamine was of interest because it is a possible precursor of 1,2-ethanediol (ethylene glycol). After solid-phase extraction the sample was derivatized with 9-fluorenylmethoxycarbonylchloride. The derivatives were separated by HPLC and detected by fluorescence spectroscopy. In musts, 3 to 8 mg/L and in wines 4 to 17 mg/L ethanolamine were determined.

引用

页码：315 / 317

页数：3

共 8 条

[1] OCCURRENCE AND ORIGIN OF VOLATILE PRIMARY AMINES IN BACTERIA [J].

BAST, E .

ARCHIV FUR MIKROBIOLOGIE, 1971, 79 (01) :7-&

[2] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETECTION AND QUANTITATION OF AMINES IN MUST AND WINE [J].

BUTEAU, C ;

DUITSCHAEVER, CL ;

ASHTON, GC .

JOURNAL OF CHROMATOGRAPHY, 1984, 284 (01) :201-210

[3] DETERMINATION OF AMINO-ACIDS WITH 9-FLUORENYLMETHYL CHLOROFORMATE AND REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].

EINARSSON, S ;

JOSEFSSON, B ;

LAGERKVIST, S .

JOURNAL OF CHROMATOGRAPHY, 1983, 282 (DEC) :609-618

[4] DEGRADATION OF DIOLS AND FORMATION OF ETHYLENE-GLYCOL BY DIFFERENT YEAST SPECIES [J].

HERZBERGER, E ;

KAPOL, R ;

PFEIFFER, P ;

RADLER, F .

ZEITSCHRIFT FUR LEBENSMITTEL-UNTERSUCHUNG UND-FORSCHUNG, 1989, 188 (04) :309-313

[5] ISOLATION AND HPLC DETERMINATION OF AMINES IN WINE [J].

LEHTONEN, P .

ZEITSCHRIFT FUR LEBENSMITTEL-UNTERSUCHUNG UND-FORSCHUNG, 1986, 183 (03) :177-181

[6]

RADLER F, 1991, PROCEEDINGS OF THE INTERNATIONAL SYMPOSIUM ON NITROGEN IN GRAPES AND WINE, P185

[7]

RENNER R, 1986, VORTRAG DTSCH LEBENS

[8] GAS-CHROMATOGRAPHIC ANALYSIS OF BACTERIAL AMINES AS THEIR FREE BASES [J].

TAVAKKOL, A ;

DRUCKER, DB .

JOURNAL OF CHROMATOGRAPHY, 1983, 274 (MAY) :37-44

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