1'-Allyl-1-(3,4-dimethylbenzoyl)-2-(4-methyl-1,3-thiazol-5-yl)-1,2,5,6,7,7a-hexahydrospiro[pyrrolizine-3,3'-indolin]2'-one

被引：0

作者：

Karthikeyan, V. ^{[1
]}

Ramkumar, V. ^{[2
]}

Karunakaran, R. Joel ^{[1
]}

机构：

[1] Madras Christian Coll, Dept Chem, Madras 600059, Tamil Nadu, India

[2] IIT Madras, Dept Chem, Madras 600036, Tamil Nadu, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

关键词：

data-to-parameter ratio = 13.7; mean σ(C-C) = 0.003 A°; R factor = 0.039; single-crystal X-ray study; T = 298 K; wR factor = 0.112;

D O I：

10.1107/S1600536814006990

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C30H31N3O2S, the fused pyrrolidine ring bearing three substituents adopts an envelope conformation with the C atom bearing the benzoyl group as the flap. The other fused pyrrolidine ring adopts a twisted conformation about one of its C-C bonds. The dihedral angle between the isatin ring system and the methylthiazole ring is 25.95 (8)degrees. An intramolecular C-H center dot center dot center dot O interaction closes an S(8) ring. In the crystal, molecules are linked by C-H center dot center dot center dot O interactions, generating C(11) chains propagating in [001].

引用

页码：O541 / +

页数：11

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