Crystal structure of 2-cyclohexyl-1,3-thiazolo[4,5-b]pyridine

被引：1

作者：

El-Hiti, Gamal A. ^{[1
]}

Smith, Keith ^{[2
]}

Hegazy, Amany S. ^{[2
]}

Ajarim, Mansour D. ^{[3
]}

Kariuki, Benson M. ^{[2
]}

机构：

[1] King Saud Univ, Dept Optometry, Coll Appl Med Sci, Cornea Res Chair, POB 10219, Riyadh 11433, Saudi Arabia

[2] Cardiff Univ, Sch Chem, Cardiff CF10 3AT, S Glam, Wales

[3] Minist Interior, Criminal Evidence, Riyadh 11632, Saudi Arabia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2015年 / 71卷

关键词：

crystal structure; cyclohexane; thiazolopyridine derivatives; thiazolo[4,5-b]pyridine;

D O I：

10.1107/S2056989015019106

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C12H14N2S, the cyclohexane ring adopts a chair conformation with the exocyclic C-C bond in an equatorial orientation. The mean plane through the cyclohexane ring (all atoms) is twisted from the thiazolopyridine ring system (r.m.s. deviation = 0.013 angstrom) by 39.57 (6)degrees. In the crystal, molecules form (100) sheets, although there are no specific directional interactions between them. The crystal stucture was refined as a two-component perfect twin.

引用

页码：O866 / +

页数：6

共 8 条

[1] [Anonymous], 2014, CRYSALIS PRO
[2] Crystal structure of 2-(1-methylethyl)-1,3-thiazolo[4,5-b]pyridine
El-Hiti, Gamal A.
Smith, Keith
Hegazy, Amany S.
Alanazi, Saud A.
Kariuki, Benson M.
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O272 - U222
[3] WinGX and ORTEP for Windows: an update
Farrugia, Louis J.
[J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2012, 45 : 849 - 854
[4] THIAZOLOPYRIDINE ANALOGS OF NALIDIXIC-ACID .2. THIAZOLO[4,5-B]PYRIDINES
LEYSEN, DC
HAEMERS, A
BOLLAERT, W
[J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 1984, 21 (05) : 1361 - 1366
[5] A short history of SHELX
Sheldrick, George M.
[J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
[6] Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053229614024218, 10.1107/S0108767307043930]
[7] SMITH K, 1995, SULFUR LETT, V18, P79
[8] Soft Cambridge, 2001, CHEMDRAW ULTR

← 1 →