X-ray absorption study of local structure in nanophase palladium

被引:1
作者
DePanfilis, S
DAcapito, F
Haas, V
Konrad, H
Weissmuller, J
Boscherini, F
机构
[1] IST NAZL FIS NUCL, LAB NAZL FRASCATI, I-00044 FRASCATI, ITALY
[2] CNR, GILDA CRG, ESRF, F-38043 GRENOBLE, FRANCE
[3] UNIV SAARLAND, D-66121 SAARBRUCKEN, GERMANY
来源
NANOPHASE MATERIALS | 1995年 / 195卷
关键词
nanophase materials; x-ray absorption spectroscopy; grain boundaries;
D O I
10.4028/www.scientific.net/MSF.195.67
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
We present an X-ray absorption study of local order in nanophase Pd deposited by inert gas evaporation. Samples were subjected to various pressure and temperature treatments and were carefully characterized by X-ray diffraction. We find that there is a reduction in the average coordination numbers in the first few coordination shells; this reduction can be reproduced by considering the surface to bulk ratio and the distribution of dimensions of the nanometer-sized particles.
引用
收藏
页码:67 / 72
页数:6
相关论文
共 27 条
[1]  
BALERNA A, 1986, PHYS REV B, V34, P2293, DOI 10.1103/PhysRevB.34.2293
[2]   TEMPERATURE AND POLARIZATION DEPENDENCE OF EXTENDED X-RAY ABSORPTION FINE-STRUCTURE SPECTRA [J].
BENI, G ;
PLATZMAN, PM .
PHYSICAL REVIEW B, 1976, 14 (04) :1514-1518
[3]  
BOSCHERINI F, 1994, FUNDAMENTAL PROPERTI
[4]  
DICICCO A, 1994, PHYS REV B, V50
[5]  
Eastman J. A., 1992, Nanostructured Materials, V1, P47, DOI 10.1016/0965-9773(92)90051-X
[6]   THE THERMAL-PROPERTIES OF NANOCRYSTALLINE PD FROM 16-K TO 300-K [J].
EASTMAN, JA ;
FITZSIMMONS, MR ;
THOMPSON, LJ .
PHILOSOPHICAL MAGAZINE B-PHYSICS OF CONDENSED MATTER STATISTICAL MECHANICS ELECTRONIC OPTICAL AND MAGNETIC PROPERTIES, 1992, 66 (05) :667-696
[7]   EXTENDED X-RAY ABSORPTION FINE-STRUCTURE DETERMINATIONS OF COORDINATION NUMBERS - LIMITATIONS [J].
EISENBERGER, P ;
LENGELER, B .
PHYSICAL REVIEW B, 1980, 22 (08) :3551-3562
[8]   STRUCTURAL CHARACTERIZATION OF NANOMETER-SIZED CRYSTALLINE PD BY X-RAY-DIFFRACTION TECHNIQUES [J].
FITZSIMMONS, MR ;
EASTMAN, JA ;
MULLERSTACH, M ;
WALLNER, G .
PHYSICAL REVIEW B, 1991, 44 (06) :2452-2460
[9]   NANOCRYSTALLINE MATERIALS [J].
BIRRINGER, R .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1989, 117 :33-43
[10]  
Gleiter H., 1981, P 2 RIS INT S MET MA