SYNTHESIS OF 2-PHENYLETHYL ALPHA-GLUCOSIDE

被引：6
作者：
SHU, CK
LAWRENCE, BM
机构：
[1] Bowman Gray Technical Center, R. J. Reynolds Tobacco Company, Winston-Salem, North Carolina 27105
来源：
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY | 1994年 / 42卷 / 08期
关键词：
2-PHENYLETHANOL; 2-PHENYLETHYL ALPHA-GLUCOSIDE; ALPHA-D-GLUCOSE; P-TOLUENESULFONIC ACID;
D O I：
10.1021/jf00044a029
中图分类号：
S [农业科学];
学科分类号：
09 ;
摘要：
2-Phenylethyl alpha-glucoside was synthesized from 2-phenylethanol and alpha-D-glucose in the presence of p-toluenesulfonic acid monohydrate at 75 degrees C and was isolated by continuous extraction, during which hexane was used to remove the excess 2-phenylethanol and then ethyl acetate was used to isolate the product. The spectral data including IR, H-1 NMR, C-13 NMR, and MS of this compound are presented.
引用
收藏
页码：1732 / 1733
页数：2
相关论文
共 16 条
  • [1] BETA-GLUCOSIDES OF AROMA COMPONENTS FROM PETALS OF ROSA SPECIES - ASSAY, OCCURRENCE, AND BIOSYNTHETIC IMPLICATIONS
    ACKERMANN, IE
    BANTHORPE, DV
    FORDHAM, WD
    KINDER, JP
    POOTS, I
    [J]. JOURNAL OF PLANT PHYSIOLOGY, 1989, 134 (05) : 567 - 572
  • [2] TOMATO AROMA COMPONENTS - IDENTIFICATION OF GLYCOSIDE HYDROLYSIS VOLATILES
    BUTTERY, RG
    TAKEOKA, G
    TERANISHI, R
    LING, LC
    [J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1990, 38 (11) : 2050 - 2053
  • [3] Campbell H. H., 1952, U.S. Patent, Patent No. [2,610,206, 2610206]
  • [4] MONO AND SESQUITERPENE ALCOHOL GLYCOSIDES .1. SYNTHESIS AND PHYSICOCHEMICAL DATA OF PRIMARY ALCOHOL-BETA-D-GLUCOPYRANOSIDES
    ISHAG, KEA
    JORK, H
    ZEPPEZAUER, M
    [J]. FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1985, 321 (04): : 331 - 336
  • [5] KODAMA H, 1984, PHYTOCHEMISTRY, V3, P583
  • [6] GLYCOSIDICALLY BOUND AROMA COMPOUNDS IN THE FRUITS OF PRUNUS SPECIES - APRICOT (PRUNUS-ARMENIACA L), PEACH (P-PERSICA, L), YELLOW PLUM (P-DOMESTICA, L SSP SYRIACA)
    KRAMMER, G
    WINTERHALTER, P
    SCHWAB, M
    SCHREIER, P
    [J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1991, 39 (04) : 778 - 781
  • [7] LEONG G, 1989, Flavour and Fragrance Journal, V4, P163, DOI 10.1002/ffj.2730040402
  • [8] MASTELIC J, 1989, Flavour and Fragrance Journal, V4, P169, DOI 10.1002/ffj.2730040403
  • [9] MIYASE T, 1988, CHEM PHARM BULL, V36, P2475, DOI 10.1248/cpb.36.2475
  • [10] GLYCOSIDIC CONJUGATES OF ALIPHATIC-ALCOHOLS FROM APPLE FRUIT (MALUS-SYLVESTRIS MILL CULT JONATHAN)
    SCHWAB, W
    SCHREIER, P
    [J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1990, 38 (03) : 757 - 763
12