9-(5-Bromo-1H-indol-3-yl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dionedimethyl sulfoxide monosolvate

被引：8

作者：

El-Khouly, Ahmed ^{[1
]}

Yildirim, Sema Ozturk ^{[2
,3
]}

Butcher, Ray J. ^{[2
]}

Simsek, Rahime ^{[1
]}

Safak, Cihat ^{[1
]}

机构：

[1] Hacettepe Univ, Fac Pharm, Dept Pharmaceut Chem, TR-06100 Ankara, Turkey

[2] Howard Univ, Dept Chem, 525 Coll St NW, Washington, DC 20059 USA

[3] Erciyes Univ, Fac Sci, Dept Phys, TR-38039 Kayseri, Turkey

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-toparameter ratio = 15.3; disorder in solvent or counterion; mean ω(C-C) = 0.004 Å; R factor = 0.052; single-crystal X-ray study; T = 123 K; wR factor = 0.137;

D O I：

10.1107/S1600536812045886

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C21H19BrN2O2 center dot C2H6OS, the indole ring system is essentially planar, with a maximum deviation of 0.050 (3) angstrom for the non-bridgehead C atom adjacent to the N atom. The two cyclohex-2-enone rings adopt half-chair conformations. An intramolecular C-H center dot center dot center dot O hydrogen bond occurs. The solvent molecule exhibits minor disorder of the S atom [site occupancies = 0.8153 (16) and 0.1847 (18)]. In the crystal, molecules are linked by N-H center dot center dot center dot O hydrogen bonds, forming layers parallel to the bc plane.

引用

页码：O3337 / +

页数：9

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