(E)-3-Methyl-N'-(4-nitrobenzylidene)-benzohydrazide methanol monosolvate

被引：0
|
作者：
Tang, Chun-Bao [1 ]
机构：
[1] Jiaying Univ, Dept Chem, Meizhou 514015, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
data-to-parameter ratio = 14.9; mean σ(C-C) = 0.004 Å; R factor = 0.058; single-crystal X-ray study; T = 298 K; wR factor = 0.142;
D O I：
10.1107/S1600536812003868
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title hydrazone compound, C 15H 13N 3O3·CH 3OH, crystallized as a methanol solvate. The hydrazone molecule has an E configuration about the C=N bond and is almost planar, with a dihedral angle between the benzene rings of 5.3 (3)°. In the crystal, the hydrazone molecules are linked via the methanol solvent molecule through N - H⋯O and O - H⋯O hydrogen bonds, so forming chains propagating along the a-axis direction.
引用
收藏
页码：O602 / U1398
页数：7
相关论文
共 50 条
  • [31] 4-Methoxy-N '-(3-nitrobenzylidene)benzohydrazide
    Hou, Jin-Long
    Bi, Ye
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1725 - +
  • [32] 2,3-Dimethyl-N-[(E)-4-nitrobenzylidene]aniline
    Tariq, Muhammad Ilyas
    Ahmad, Shahbaz
    Tahir, M. Nawaz
    Sarfaraz, Muhammad
    Hussain, Ishtiaq
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2010, 66 : O1561 - U470
  • [33] N '-(3,5-Dichloro-2-hydroxybenzylidene)-4-(dimethylamino)benzohydrazide methanol monosolvate
    Xu, Huanzhi
    Sun, Jingya
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1042 - +
  • [34] Synthesis,Crystal Structure,and Antioxidant and Antibacterial Activities of3,5-Dihydroxy-N'-(4-nitrobenzylidene)benzohydrazide
    计建军
    黄珊珊
    张厚利
    林原
    李坤
    刁云鹏
    结构化学, 2013, 32 (10) : 1523 - 1529
  • [35] 4-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvate
    Zhi, Feng
    Wang, Rong
    Zhang, Yi
    Wang, Qiang
    Yang, Yi-Lin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2825 - +
  • [36] 4-Dimethylamino-N '-(2-hydroxy4-methoxybenzylidene)benzohydrazide methanol monosolvate
    Sun, Jingya
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2998 - +
  • [37] N′-(4-Diethylamino-2-hydroxybenzylidene)-4-(dimethylamino)benzohydrazide methanol monosolvate
    Su, Fu
    Gu, Zheng-Gui
    Lin, Jun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1634 - U230
  • [38] 4-Hydroxy-N′-(4-hydroxy-3-nitrobenzylidene)benzohydrazide
    Zhang, Zhen
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O300 - U2279
  • [39] Third-order nonlinear optical properties and structures of (E)-N-(4-nitrobenzylidene)-2,6-dimethylaniline and (E)-N-(4-nitrobenzylidene)-2,3-dimethylaniline
    Karakas, Asli
    Unver, Hueseyin
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2010, 75 (05) : 1492 - 1496
  • [40] Conformational polymorphism of (E,E)-N,N′-bis(4-nitrobenzylidene)benzene-1,4-diamine
    Collas, Alain
    Zeller, Matthias
    Blockhuys, Frank
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2011, 67 : O171 - O174
12345