ORGANOMETALLOIDAL COMPOUNDS WITH O-PHENYLENE-SUBSTITUENTS, .27. SYNTHESIS, CHARACTERIZATION AND STRUCTURE DETERMINATION OF 2,3,7,8-TETRAKIS(METHYLTHIO) THIANTHRENE AND 2,3,7,8-BIS(ETHYLENEDITHIO) THIANTHRENE

被引：13

作者：

DOTZE, M ^{[1
]}

KLAR, G ^{[1
]}

机构：

[1] UNIV HAMBURG,INST ANORGAN & ANGEW CHEM,MARTIN LUTHER KING PLATZ 6,D-20146 HAMBURG,GERMANY

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 1993年 / 84卷 / 1-4期

关键词：

2,3,7,8-TETRAKIS(ALKYLTHIO)THIANTHRENES; SYNTHESIS; 2,3,7,8-TETRAKIS(METHYLTHIO) AND 2, 3; 7,8-BIS(ETHYLENDITHIO)THIANTHRENE; H-1-NMR; MS; CV-DATA; X-RAY STRUCTURES;

D O I：

10.1080/10426509308034319

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A generally applicable synthesis via the sequence thiophenol (3),1,2-bis(alkylthio)benzene (6), 1-bromo-3,4-bis(alkykthio)benzene (7), bis[3,4-bis(alkylthio)phenyl]sulfide (8), bis[2-bromo-4,5-bis(alkylthio)-pheny]sulfide (9), 2,3,7,8-tetrakis(alkylthio)thianthrene (2) has been worked out for the title compounds. Their H-1-NMR, MS and CV data are given, the results of the crystal structure determinations as well.

引用

页码：95 / 106

页数：12

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