ORGANOMETALLOIDAL COMPOUNDS WITH O-PHENYLENE-SUBSTITUENTS, .27. SYNTHESIS, CHARACTERIZATION AND STRUCTURE DETERMINATION OF 2,3,7,8-TETRAKIS(METHYLTHIO) THIANTHRENE AND 2,3,7,8-BIS(ETHYLENEDITHIO) THIANTHRENE

被引：13
|
作者：
DOTZE, M [1 ]
KLAR, G [1 ]
机构：
[1] UNIV HAMBURG,INST ANORGAN & ANGEW CHEM,MARTIN LUTHER KING PLATZ 6,D-20146 HAMBURG,GERMANY
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 1993年 / 84卷 / 1-4期
关键词：
2,3,7,8-TETRAKIS(ALKYLTHIO)THIANTHRENES; SYNTHESIS; 2,3,7,8-TETRAKIS(METHYLTHIO) AND 2, 3; 7,8-BIS(ETHYLENDITHIO)THIANTHRENE; H-1-NMR; MS; CV-DATA; X-RAY STRUCTURES;
D O I：
10.1080/10426509308034319
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A generally applicable synthesis via the sequence thiophenol (3),1,2-bis(alkylthio)benzene (6), 1-bromo-3,4-bis(alkykthio)benzene (7), bis[3,4-bis(alkylthio)phenyl]sulfide (8), bis[2-bromo-4,5-bis(alkylthio)-pheny]sulfide (9), 2,3,7,8-tetrakis(alkylthio)thianthrene (2) has been worked out for the title compounds. Their H-1-NMR, MS and CV data are given, the results of the crystal structure determinations as well.
引用
收藏
页码：95 / 106
页数：12
相关论文
共 25 条
  • [1] Synthesis of 2,3,7,8-tetrakis(alkylthio)dibenzothiophenes and structure of 2,3,7,8-tetrakis(methylthio)dibenzothiophene
    Dotze, M
    Klar, G
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1996, 117 : 197 - 203
  • [2] ORGANOELEMENT COMPOUNDS WITH ORTHO-PHENYLENE SUBSTITUENTS .20. 2,3,7,8-TETRA(METHYLTHIO)THIANTHRENE
    DOTZE, M
    KLAR, G
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1991, 63 (1-2): : 217 - 222
  • [3] Organometalloidal compounds with o-phenylene substituents, part XXXI.: Charge-transfer complexes of 2,3,7,8-tetrakis(methylthio)chalkogenanthrenes with 7,7,8,8-tetracyanoquinodimethane and tetracyanoethene
    Dötze, M
    Czepat, H
    Kudnig, J
    Klar, G
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1998, 53 (11): : 1316 - 1322
  • [4] Organometalloidal Compounds with o-Phenylene Substituents, Part XXXI [1]. Charge-transfer Complexes of 2,3,7,8-Tetrakis(methylthio)chalkogenanthrenes with 7,7,8,8-Tetracyanoquinodimethane and Tetracyanoethene
    Dötze, Marc
    Czepat, Hendrik
    Kudnig, Jens
    Klar, Günter
    Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1998, 53 (11): : 1316 - 1322
  • [5] ORGANOMETALLOIDAL COMPOUNDS WITH ORTHO-PHENYLENE SUBSTITUENTS .13. CRYSTAL AND MOLECULAR-STRUCTURE OF 2,3,7,8-TETRAMETHOXYSELENANTHRENE
    SCHIFFLING, C
    KLAR, G
    JOURNAL OF CHEMICAL RESEARCH-S, 1987, (08): : 248 - 249
  • [6] THE STRUCTURE AND REACTIVITY OF 2,3,7,8-TETRAKIS(TRIMETHYLSILYL)TERPHENYLENE, A NOVEL LINEAR MULTIPHENYLENE
    HOVAKEEMIAN, GH
    VOLLHARDT, KPC
    ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1983, 22 (12): : 994 - 996
  • [7] ORGANOMETALLOIDAL COMPOUNDS WITH ORTHO-PHENYLENE SUBSTITUENTS .25. CRYSTAL AND MOLECULAR-STRUCTURES OF 2,3,7,8-TETRAHYDROXYTHIANTHRENE
    MANSEL, V
    KLAR, G
    JOURNAL OF CHEMICAL RESEARCH-S, 1992, (05): : 158 - 159
  • [8] ORGANOMETALLOIDAL COMPOUNDS WITH ORTHO-PHENYLENE SUBSTITUENTS .21. CRYSTAL AND MOLECULAR-STRUCTURES OF THE TETRAGONAL FORMS OF 2,3,7,8-TETRAMETHOXYSELENANTHRENE AND OF 2,3,7,8-TETRAMETHOXYDIBENZO[B,E][1,4]THIASELENINE
    DOTZE, M
    HINRICHS, W
    KLAR, G
    JOURNAL OF CHEMICAL RESEARCH-S, 1991, (11): : 314 - 315
  • [9] ORGANOMETALLIC COMPOUNDS WITH O-PHENYLENE SUBSTITUENTS .8. CRYSTAL AND MOLECULAR-STRUCTURE OF 2,3,7,8-TETRA-METHOXYTHIANTHRENE
    HINRICHS, W
    RIEDEL, HJ
    KLAR, G
    JOURNAL OF CHEMICAL RESEARCH-S, 1982, (12): : 334 - 335
  • [10] Organometalloidal compounds with o-phenylene substituents .28. Charge-transfer complexes of 2,3,7,8-tetraalkoxy-chalcogenanthrenes with 7,7,8,8-tetracyano-2,3,5,6-tetrafluoro-quinodimethane
    Friederichs, S
    Kudnig, J
    Klar, G
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1996, 51 (09): : 1295 - 1300
123