USE OF SODIUM TETRAETHYLBORATE FOR THE ANALYSIS OF TRIMETHYLLEAD SPECIES IN ARTIFICIAL RAINWATER AND A NATURAL ROAD DUST SAMPLE

被引:15
作者
CRAIG, PJ
DEWICK, RJ
VANELTEREN, JT
机构
[1] Department of Chemistry, De Montfort University, Leicester, LE1 9BH, The Gateway
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1995年 / 351卷 / 4-5期
关键词
D O I
10.1007/BF00322921
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Several artificial rainwater samples and a natural sample of road dust have been analysed for trimethyl-lead under the aegis of a European Union Measurement and Testing (Bureau of Community Reference - BCR) intercomparison exercise, using a new and simplified purge and trap ethylation technique. Levels of trimethyllead found have been similar to those reported at lower levels from the natural environment. The method has been successful in the presence of excess amounts of inorganic lead, even for organic lead levels one tenth of those recently reported for the natural environment.
引用
收藏
页码:467 / 470
页数:4
相关论文
共 22 条
[1]   NEW METHOD FOR THE PRODUCTION OF VOLATILE ORGANOMETALLIC SPECIES FOR ANALYSIS FROM THE ENVIRONMENT - SOME BUTYL TIN LEVELS IN UK SEDIMENTS [J].
ASHBY, JR ;
CRAIG, PJ .
SCIENCE OF THE TOTAL ENVIRONMENT, 1989, 78 :219-232
[2]   SPECIATION FOR ANALYSIS OF ORGANOTIN COMPOUNDS BY GC AA AND GC MS AFTER ETHYLATION BY SODIUM TETRAETHYLBORATE [J].
ASHBY, JR ;
CRAIG, PJ .
APPLIED ORGANOMETALLIC CHEMISTRY, 1991, 5 (03) :173-181
[3]   POST-COLUMN ETHYLATION FOR THE DETERMINATION OF IONIC ALKYLLEAD COMPOUNDS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY ATOMIC-ABSORPTION SPECTROMETRY [J].
BLAIS, JS ;
MARSHALL, WD .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1989, 4 (07) :641-645
[5]   ETHYLATION OF METHYLARSENIC(III) COMPOUNDS BY SODIUM TETRAETHYLBORATE [J].
CLAMAGIRAND, V ;
MARR, IL ;
WARDELL, JL .
APPLIED ORGANOMETALLIC CHEMISTRY, 1993, 7 (07) :577-581
[6]   THE USE OF SODIUM TETRAETHYLBORATE FOR THE DERIVATIZATION AND ANALYSIS OF SELENIUM CONTAINING COMPOUNDS [J].
CLARK, S ;
CRAIG, PJ .
MIKROCHIMICA ACTA, 1992, 109 (1-4) :141-144
[7]   NUCLEAR-MAGNETIC-RESONANCE AND MASS-SPECTRA OF ORGANOMERCURY HYDRIDES AND DEUTERIDES .2. [J].
CRAIG, PJ ;
GARRAUD, H ;
LAURIE, SH ;
MENNIE, D ;
STOJAK, GH .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1994, 468 (1-2) :7-11
[8]  
EDBON L, 1993, J ANAL ATOM SPECTROM, V8, P723
[9]   TRIORGANOBORANES AS ALKYLATING AGENTS [J].
HONEYCUTT, JB ;
RIDDLE, JM .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1960, 82 (12) :3051-3052
[10]  
LOBINSKI R, 1992, ANAL CHIM ACTA, V262, P285