2-(cyclohex-2-enyloxy)-isoindole-1,3-dione

被引：0

作者：

Coseri, Sergiu ^{[1
,2
]}

机构：

[1] Inst Macromol Chem P Poni Iasi, Gr Ghica Voda,41A, Iasi 6600, Romania

[2] Natl Res Council Canada, Ottawa, ON K1A 0R6, Canada

来源：

MOLBANK | 2006年 / 01期

关键词：

D O I：

10.3390/M460

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A degassed mixture containing 0.245 mmol cyclohexene and 0.05 mmol N-hydroxyphthalimide (NHPI),1,2 in 5 mL acetonitrile was added to a degassed solution of lead tetraacetate3 (0.025 mmol in 5 mL acetonitrile) under nitrogen atmosphere at room temperature. After the completion of the reaction, the solvent and the olefin excess was removed under reduced pressure and the residue was purified by preparative TLC using hexane:ethyl acetate = 2:1 as eluent, giving the above product. © 2006 MDPI. All rights reserved.

引用

页数：1

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