Interlaboratory tests of paving grade bitumen and polymer modified bitumen

被引:1
|
作者
Blazejowski, Krzysztof [1 ,3 ]
Wojcik-Wisniewska, Marta [1 ,3 ]
Olszacki, Jacek [2 ,4 ]
Peciakowski, Hubert [2 ,5 ]
机构
[1] ORLEN Asfalt Spzoo, Plock, Poland
[2] PKN ORLEN SA, Plock, Poland
[3] ORLEN Asphalt LLC, Dept Res & Dev, Res & Dev, 39 Lukasiewicz St, PL-09400 Plock, Poland
[4] PKN ORLEN SC, Dept Res & Dev, New Technol ORLEN Capital Grp, 7 Chemikow St, PL-09411 Plock, Poland
[5] PKN ORLEN SC, Refinery Optimizat & Petrochem Prod Proc Team, Field Refinery Prod, 7 Chemikow St, PL-09411 Plock, Poland
来源
NAFTA-GAZ | 2016年 / 72卷 / 05期
关键词
interlaboratory tests; round-robin tests; paving grade bitumen; polymer modified bitumen; statistical evaluation;
D O I
10.18668/NG.2016.05.07
中图分类号
TE [石油、天然气工业];
学科分类号
0820 ;
摘要
In the paper the results of interlaboratory round-robin tests are presented. The RR program was executed for paving grade 50/70 bitumen and polymer modified bitumen 45/80-55. For both binders similar test programs have been prepared, starting from fundamental properties like Pen@25, Softening Point, Softening Point after RTFOT, Fraass breaking point, elastic recovery etc. and with use of more contemporary test methods as complex modulus G*, phase angle delta(60 degrees C, f = 1.59 Hz (10 rad/s), PMB microstructure etc. Finally 8 properties for unmodified bitumen were tested and 9 for PMBs. In the program 24 laboratories from three european countries participated representing different kinds of labs - private owned, technical universities, road administration and refinery control labs. The final results were evaluated with statistical and z-score method. Surprisingly results showed that the best methods with high reproductibility are complex modulus G* and phase angle d.
引用
收藏
页码:356 / 363
页数:8
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