Thermal analysis, X-ray powder diffraction and electron microscopy data related with the production of 1:1 Caffeine:Glutaric Acid cocrystals

被引：2

作者：

Duarte, Iris ^{[1
,2
]}

Andrade, Rita ^{[2
]}

Pinto, Joao F. ^{[1
]}

Temtem, Marcio ^{[2
]}

机构：

[1] Univ Lisbon, Fac Pharm, Res Inst Med iMed ULisboa, Lisbon, Portugal

[2] Hovione Farmaciencia SA, R&D Drug Prod Dev, Loures, Portugal

来源：

DATA IN BRIEF | 2016年 / 8卷

关键词：

D O I：

10.1016/j.dib.2016.04.074

中图分类号：

O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];

学科分类号：

07 ; 0710 ; 09 ;

摘要：

The data presented in this article are related to the production of 1:1 Caffeine:Glutaric Acid cocrystals as part of the research article entitled "Green production of cocrystals using a new solvent-free approach by spray congealing" (Duarte et al., 2016) [1]. More specifically, here we present the thermal analysis and the X-ray powder diffraction data for pure Glutaric Acid, used as a raw material in [1]. We also include the X-ray powder diffraction and electron microscopy data obtained for the 1:1 Caffeine:Glutaric Acid cocrystal (form II) produced using the cooling crystallization method reported in "Operating Regions in Cooling Cocrystallization of Caffeine and Glutaric Acid in Acetonitrile" (Yu et al., 2010) [2]. Lastly, we show the X-ray powder diffraction data obtained for assessing the purity of the 1:1 Caffeine:Glutaric cocrystals produced in [1]. (C) 2016 The Authors. Published by Elsevier Inc. This is an open access article under the CC BY license

引用

页码：247 / 250

页数：4

共 2 条

[1] Green production of cocrystals using a new solvent-free approach by spray congealing [J].

Duarte, Iris ;

Andrade, Rita ;

Pinto, Joao F. ;

Temtem, Marcio .

INTERNATIONAL JOURNAL OF PHARMACEUTICS, 2016, 506 (1-2) :68-78

[2] Operating Regions in Cooling Cocrystallization of Caffeine and Glutaric Acid in Acetonitrile [J].

Yu, Zai Qun ;

Chow, Pui Shan ;

Tan, Reginald B. H. .

CRYSTAL GROWTH & DESIGN, 2010, 10 (05) :2382-2387

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