HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC SEPARATION OF POTATO GLYCOALKALOIDS

被引：50

作者：

BUSHWAY, RJ

BARDEN, ES

BUSHWAY, AW

BUSHWAY, AA

机构：

[1] Department of Food Science, University of Maine, Orono

来源：

JOURNAL OF CHROMATOGRAPHY | 1979年 / 178卷 / 02期

关键词：

D O I：

10.1016/S0021-9673(00)92512-3

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Separations of three glycoalkaloids (a-chaconine, β-chaconine, and a-solanine) have been achieved by using three different columns: μBondapak C18, μBondapak NH2, and a carbohydrate analysis column. These methods have been employed to examine the purity of the potato glycoalkaloids isolated by thin-layer and column chromatographic separations. Also, samples of tubers, peels, blossoms, and sprouts have been analyzed to determine their content of a-chaconine, β-chaconine, and a-solanine by using the carbohydrate and μBondapak NH2 columns. © 1979.

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页码：533 / 541

页数：9

相关论文

共 18 条

[1] TERATOGENICITY STUDIES ON LATE BLIGHTED POTATOES IN NONHUMAN-PRIMATES (MACACA-MULATTA AND SAGUINUS-LABIATUS) [J].

ALLEN, JR ;

MARLAR, RJ ;

CHESNEY, CF ;

HELGESON, JP ;

KELMAN, A ;

WECKEL, KG ;

TRAISMAN, E ;

WHITE, JW .

TERATOLOGY, 1977, 15 (01) :17-23

[2] METHOD FOR RAPID ESTIMATION OF GLYCOALKALOIDS IN POTATO TUBERS [J].

BRETZLOFF, CW .

AMERICAN POTATO JOURNAL, 1971, 48 (05) :158-+

[3]

DABBS D. H., 1953, CANADIAN JOUR TECHNOL, V31, P213

[4] COMPREHENSIVE METHOD FOR DETERMINATION OF TOTAL POTATO GLYCOALKALOIDS [J].

FITZPATRICK, TJ ;

OSMAN, SF .

AMERICAN POTATO JOURNAL, 1974, 51 (10) :318-323

[5] Two fatal cases of potato poisoning [J].

Hansen, AA .

SCIENCE, 1925, 61 :340-341

[6] SEPARATION OF POTATO GLYCOALKALOIDS BY GAS-CHROMATOGRAPHY [J].

HERB, SF ;

FITZPATRICK, TJ ;

OSMAN, SF .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1975, 23 (03) :520-523

[7] HIGH-PRESSURE LIQUID-CHROMATOGRAPHY OF STEROIDAL ALKALOIDS [J].

HUNTER, IR ;

WALDEN, MK ;

WAGNER, JR ;

HEFTMANN, E .

JOURNAL OF CHROMATOGRAPHY, 1976, 119 (APR28) :223-226

[8] TERATOGENICITY OF SOLANUM ALKALOID SOLASODINE AND OF KENNEBEC POTATO SPROUTS IN HAMSTERS [J].

KEELER, RF ;

BROWN, D ;

DOUGLAS, DR ;

STALLKNECHT, GF ;

YOUNG, S .

BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 1976, 15 (05) :522-524

[9] TESTING OF BLIGHTED, AGED, AND CONTROL RUSSET BURBANK POTATO-TUBER PREPARATION FOR ABILITY TO PRODUCE SPINA-BIFIDA AND ANENCEPHALY IN RATS, RABBITS, HAMSTERS, AND MICE [J].

KEELER, RF ;

DOUGLAS, DR ;

STALLKNECHT, GF .

AMERICAN POTATO JOURNAL, 1975, 52 (04) :125-132

[10] EVALUATION OF A COMPREHENSIVE METHOD FOR TOTAL GLYCOALKALOID DETERMINATION [J].

MACKENZIE, JD ;

GREGORY, P .

AMERICAN POTATO JOURNAL, 1979, 56 (01) :27-33