6-[(2-Chloropyridin-5-ylmethyl)(ethyl)-azanyl]-4-(2-fluorophenyl)-1-methyl-5-nitro-1,2,3,4-tetrahydropyridin-2-one

被引:0
作者
Sun, Chuan-Wen [1 ]
Wang, Jing [1 ]
Wu, Ying [1 ]
机构
[1] Shanghai Normal Univ, Coll Life & Environm Sci, Dept Chem, Shanghai 200234, Peoples R China
基金
中国国家自然科学基金;
关键词
data-to-parameter ratio = 12.8; mean σ(C-C) = 0.005 Å; R factor = 0.070; single-crystal X-ray study; T = 298 K; wR factor = 0.151;
D O I
10.1107/S1600536812005776
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C 20H 20ClFN 4O 3, the tetra-hydro-pyridone ring adopts a skew boat conformation. The dihedral angle between the mean planes of the benzene and pyridine rings is 80.7 (3)°. In the crystal, weak C - H⋯O inter-actions are observed.
引用
收藏
页码:O753 / U2390
页数:9
相关论文
共 50 条
[41]   2-(4-Fluorophenyl)-5-iodo-3-isopropylsulfonyl-1-benzofuran [J].
Choi, Hong Dae ;
Seo, Pil Ja ;
Lee, Uk .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O3192-+
[42]   5-Cyclopentyl-2-(4-fluorophenyl)-3isopropylsulfonyl-1-benzofuran [J].
Choi, Hong Dae ;
Seo, Pil Ja ;
Lee, Uk .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O3336-+
[43]   (6Z)-3,5-Bis(4-fluorophenyl)-6-(1-hydroxyethylidene)cyclohex-2-en-1-one [J].
Jasinski, Jerry P. ;
Golen, James A. ;
Samshuddin, S. ;
Narayana, B. ;
Yathirajan, H. S. .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O638-U1648
[44]   N-[4-(4-Fluorophenyl)-5-hydroxymethyl-6-isopropylpyrimidin-2-yl]-N-methylmethanesulfonamide [J].
Xu, Hong ;
Sun, Hong-shun ;
Luo, Feng-mao .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O3432-U2025
[45]   2-[5-(2-Methylphenyl)-3-(2-methylstyryl)-4,5-dihydro-1H-pyrazol-1-yl]-6-(thiophen-2-yl)-4-(trifluoromethyl) pyrimidine chloroform monosolvate [J].
Claro Flores, Alex Fabiani ;
Flores, Darlene Correia ;
de Menezes Vicenti, Juliano Rosa ;
Campos, Patrick Teixeira .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 :0789-+
[46]   (Z)-4-[(2-Aminoanilino)(phenyl)methylidene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one [J].
Lu, Rong ;
Xia, Hua ;
Lu, Xingqiang ;
Zhao, Shunsheng .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O2701-+
[47]   4-[Bis(4-fluorophenyl)methyl]-1-[(2E)-3-phenylprop-2-en-1-yl]piperazin-1-ium3-carboxypropanoate [J].
Kavitha, Channappa N. ;
Yathirajan, Hemmige S. ;
Narayana, Badiadka ;
Gerber, Thomas ;
van Brecht, Benjamin ;
Betz, Richard .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 :O260-+
[48]   {4-[(2,4-Dichlorobenzoyloxy)methyl]-1-phenyl-1H-1,2,3-triazol-5-yl}methyl 2,4-dichlorobenzoate [J].
Ismatov, Dilmurot ;
Azizov, Umarkhon ;
Talipov, Samat ;
Ashurov, Jamshid .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O2590-U2003
[49]   Ethyl 4-hydroxy-1-methyl-5-oxo-2-phenylpyrrolidine-3-carboxylate 1.25-hydrate [J].
Mansor, Nurul Shulehaf ;
Mohammat, Mohd Fazli ;
Shaameri, Zurina ;
Khaledi, Hamid .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 :O293-+
[50]   12-{[4-(2-Fluorophenyl)piperazin-1-yl]-methyl}-9 alpha-hydroxy-4,8-dimethyl-3,14-dioxatricyclo[9.3.0.0(2,4)]tetradec-7-en-13-one [J].
Moumou, Mohamed ;
Benharref, Ahmed ;
Daran, Jean Claude ;
Outouch, Rachid ;
Berraho, Moha .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O741-U2307