6-[(2-Chloropyridin-5-ylmethyl)(ethyl)-azanyl]-4-(2-fluorophenyl)-1-methyl-5-nitro-1,2,3,4-tetrahydropyridin-2-one

被引：0
作者：
Sun, Chuan-Wen [1 ]
Wang, Jing [1 ]
Wu, Ying [1 ]
机构：
[1] Shanghai Normal Univ, Coll Life & Environm Sci, Dept Chem, Shanghai 200234, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
基金：
中国国家自然科学基金;
关键词：
data-to-parameter ratio = 12.8; mean σ(C-C) = 0.005 Å; R factor = 0.070; single-crystal X-ray study; T = 298 K; wR factor = 0.151;
D O I：
10.1107/S1600536812005776
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C 20H 20ClFN 4O 3, the tetra-hydro-pyridone ring adopts a skew boat conformation. The dihedral angle between the mean planes of the benzene and pyridine rings is 80.7 (3)°. In the crystal, weak C - H⋯O inter-actions are observed.
引用
收藏
页码：O753 / U2390
页数：9
相关论文
共 50 条
[21]   1-[(Cyclopropylmethoxy)methyl]-6-(3,4-dimethoxybenzyl)-5-ethyl-1,2,3,4-tetrahydropyrimidine-2,4-dione ethanol hemisolvate [J].
El-Brollosy, Nasser R. ;
El-Emam, Ali A. ;
Al-Deeb, Omar A. ;
Ng, Seik Weng .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 :O349-U176
[22]   3-[2-Cyclopropyl-1-(2-fluorophenyl)-2-oxoethyl]-5-(4-methylsulfanylbenzyl-idene)-1,3-thiazolidine-2,4-dione [J].
Suresh, J. ;
Venkateshan, M. ;
Ponnuchamy, S. ;
Kumar, R. Ranjith ;
Lakshman, P. L. Nilantha .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 :O188-+
[23]   3-(4-Bromophenylsulfonyl)-5-ethyl-2-methyl-1-benzofuran [J].
Choi, Hong Dae ;
Seo, Pil Ja ;
Lee, Uk .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O3487-+
[24]   (Z)-4-(2-Hydroxybenzylidene)-1-methyl-2-phenyl-1H-imidazol-5(4H)-one [J].
Chang, Ming-Jen ;
Tsai, Hsing-Yang ;
Fang, Tzu-Chien ;
Luo, Ming-Hui ;
Chen, Kew-Yu .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O902-U3411
[25]   3-Ethyl-4-methyl-1H-pyrazol-2-ium-5-olate [J].
Rathore, R. S. ;
Narasimhamurthy, T. ;
Ragavan, R. Venkat ;
Vijayakumar, V. ;
Sarveswari, S. .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O2129-U1355
[26]   4-{[2-(2,4-Dinitrophenyl)hydrazinylidene](phenyl)methyl}-5-methyl-2phenyl-1H-pyrazol-3(2H)-one ethanol monosolvate [J].
Idemudia, Omoruyi G. ;
Sadimenko, Alexander P. ;
Hosten, Eric C. .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O3380-+
[27]   6-Ethyl-N-methyl-3-nitro-4-nitromethyl-4H-chromen-2-amine [J].
Muthukumaran, J. ;
Parthiban, A. ;
Rao, H. Surya Prakash ;
Krishna, R. .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 :o180-o181
[28]   4-[(5-Chloro-2-hydroxybenzylidene)amino]-3-ethyl-1H-1,2,4-triazole-5(4H)thione [J].
Yuan, Cai-Xia ;
Yao, Xu-Mei ;
Zhu, Miao-Li ;
Zhu, Hong-Mei .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 :O574-+
[29]   4-(4-Chlorophenyl)-8-methyl-2-oxo-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile [J].
Asiri, Abdullah M. ;
Al-Youbi, Abdulrahman O. ;
Faidallah, Hassan M. ;
Badahdah, Khadija O. ;
Ng, Seik Weng .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O2596-U2066
[30]   5-(4-Chlorophenoxy)-1-methyl-3-trifluoromethyl-1H-pyrazole-4-carbaldehyde O-[(2-chloropyridin-5-yl)methyl]oxime [J].
Dai, Hong ;
Zhu, Peng-Fei ;
Zhu, Yu-Jun ;
Fang, Jian-Xin ;
Shi, Yu-Jun .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O3246-U986
12345