LI-6 N-15 NMR-BASED SOLUTION STRUCTURAL DETERMINATION OF ET(2)O- AND TMEDA-SOLVATED LITHIOPHENYLACETONITRILE AND A LIHMDS MIXED AGGREGATE

被引：57

作者：

CARLIER, PR ^{[1
]}

LUCHT, BL ^{[1
]}

COLLUM, DB ^{[1
]}

机构：

[1] CORNELL UNIV,ITHACA,NY 14850

来源：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 1994年 / 116卷 / 25期

关键词：

D O I：

10.1021/ja00104a064

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

[No abstract available]

引用

页码：11602 / 11603

页数：2

共 33 条

[11] SOLUTION STRUCTURES OF LITHIUM DIALKYLAMIDES AND RELATED N-LITHIATED SPECIES - RESULTS FROM LI-6-N-15 DOUBLE-LABELING EXPERIMENTS [J].

COLLUM, DB .

ACCOUNTS OF CHEMICAL RESEARCH, 1993, 26 (05) :227-234

[12] STRUCTURAL STUDY AND REACTIVITY OF CARBANIONS IN SOLUTION - PHENYLACETONITRILES AND 3-PYRIDYLACETONITRILES [J].

CROISAT, D ;

SEYDENPENNE, J ;

STRZALKO, T ;

WARTSKI, L ;

CORSET, J ;

FROMENT, F .

JOURNAL OF ORGANIC CHEMISTRY, 1992, 57 (24) :6435-6447

[13] DO THE COMPOUNDS PHCH2Y GIVE GEMINAL DIANIONS ON ADDITION OF 2 EQUIVALENTS OF STRONG BASE [J].

CROWLEY, PJ ;

LEACH, MR ;

METHCOHN, O ;

WAKEFIELD, BJ .

TETRAHEDRON LETTERS, 1986, 27 (25) :2909-2912

[14] MONOLITHIUM DERIVATIVES OF ACETONITRILE AND PHENYLACETONITRILE [J].

DAS, R ;

WILKIE, CA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1972, 94 (13) :4555-&

[15] STRUCTURE AND REACTIVITY OF LITHIUM DIISOPROPYLAMIDE (LDA) - THE CONSEQUENCES OF AGGREGATION AND SOLVATION DURING THE METALATION OF AN N,N-DIMETHYLHYDRAZONE [J].

GALIANOROTH, AS ;

COLLUM, DB .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1989, 111 (17) :6772-6778

[16] LI-6, C-13, AND N-15 NMR SPECTROSCOPIC STUDIES OF LITHIUM DIALKYLAMIDES - SOLUTION STRUCTURE OF LITHIUM ISOPROPYLCYCLOHEXYLAMIDE (LICA) IN TETRAHYDROFURAN [J].

GALIANOROTH, AS ;

MICHAELIDES, EM ;

COLLUM, DB .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1988, 110 (08) :2658-2660

[17] LI-6-N-15 HETERONUCLEAR MULTIPLE QUANTUM CORRELATION (HMQC) SPECTROSCOPY - APPLICATION TO THE STRUCTURE DETERMINATION OF LITHIUM 2,2,6,6-TETRAMETHYLPIPERIDIDE MIXED AGGREGATES [J].

GILCHRIST, JH ;

HARRISON, AT ;

FULLER, DJ ;

COLLUM, DB .

MAGNETIC RESONANCE IN CHEMISTRY, 1992, 30 (09) :855-859

[18] DISTINCTION OF SYMMETRICAL LITHIUM DIALKYLAMIDE DIMERS FROM HIGHER OLIGOMERS BY INVERSE-DETECTED N-15 HOMONUCLEAR ZERO-QUANTUM NMR-SPECTROSCOPY [J].

GILCHRIST, JH ;

COLLUM, DB .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (02) :794-795

[19] STRUCTURES OF ORGANONITROGEN LITHIUM COMPOUNDS - RECENT PATTERNS AND PERSPECTIVES IN ORGANOLITHIUM CHEMISTRY [J].

GREGORY, K ;

SCHLEYER, PV ;

SNAITH, R .

ADVANCES IN INORGANIC CHEMISTRY, 1991, 37 :47-142

[20] BONDING CHARACTERISTICS OF ALKALI-METAL AMIDES IN SOLUTION AND IN THE SOLID-STATE - NMR AND X-RAY-DIFFRACTION STUDY OF N-LITHIOINDOLE N,N,N',N'-TETRAMETHYLETHYLENEDIAMINE, N-SODIOINDOLE N,N,N',N'-TETRAMETHYLETHYLENEDIAMINE, AND N-SODIOINDOLE N,N,N',N'',N''-PENTAMETHYLDIETHYLENETRIAMINE [J].

GREGORY, K ;

BREMER, M ;

BAUER, W ;

SCHLEYER, PV ;

LORENZEN, NP ;

KOPF, J ;

WEISS, E .

ORGANOMETALLICS, 1990, 9 (05) :1485-1492

← 1 2 3 4 →