N-(N-BUTYLAMIDE) OF (S)-2-(PHENYLCARBAMOYLOXY)PROPIONIC ACID - A NEW CHIRAL SOLVATING AGENT, DERIVED FROM L-LACTIC ACID, FOR THE ENANTIOMERIC PURITY DETERMINATION OF DERIVATIZED AMINO-ACIDS

被引：5

作者：

PINI, D ^{[1
]}

UCCELLOBARRETTA, G ^{[1
]}

ROSINI, C ^{[1
]}

SALVADORI, P ^{[1
]}

机构：

[1] CNR,CTR STUDIO MACROMOLEC STEREORDINATE & OTTICAMENTE ATT,DIPARTIMENTO CHIM & CHIM IND,I-56126 PISA,ITALY

来源：

CHIRALITY | 1991年 / 3卷 / 03期

关键词：

CHIRAL; CHIRAL SOLVATING AGENT; STEREOCHEMISTRY;

D O I：

10.1002/chir.530030306

中图分类号：

R914 [药物化学];

学科分类号：

100701 ;

摘要：

The N-(n-butylamide) of (S)-2-(phenylcarbamoyloxy)propionic acid, easily prepared starting from the inexpensive L-ethyl lactate, can be used as convenient chiral solvating agent (CSA) to determine the enantiomeric composition of N-(3,5-dinitrobenzoyl)amino acid methyl esters.

引用

页码：174 / 176

页数：3

共 4 条

[1] CHIRAL STATIONARY PHASE DERIVED FROM L-LACTIC ACID FOR THE OPTICAL RESOLUTION OF N-(3,5-DINITROBENZOYL)AMINO ACID METHYL-ESTERS
SALVADORI, P
PINI, D
ROSINI, C
UCCELLOBARRETTA, G
BERTUCCI, C
JOURNAL OF CHROMATOGRAPHY, 1988, 450 (02): : 163 - 168
[2] LARGE-SCALE SYNTHESIS OF THE BIFUNCTIONAL CHELATING AGENT 2-(P-NITROBENZYL)-1,4,7,10-TETRAAZACYCLODODECANE-N,N',N',N'''-TETRAACETIC ACID, AND THE DETERMINATION OF ITS ENANTIOMERIC PURITY BY CHIRAL CHROMATOGRAPHY
RENN, O
MEARES, CF
BIOCONJUGATE CHEMISTRY, 1992, 3 (06) : 563 - 569
[3] A SPECTROSCOPIC STUDY OF THE INTERACTION OF D-N-(3,5-DINITROBENZOYL)VALINE AND L-N-(3,5-DINITROBENZOYL)VALINE METHYL-ESTER WITH NORMAL-BUTYLAMIDE OF (S)-2-[(PHENYLCARBAMOYL)OXY]PROPIONIC ACID - DIRECT EVIDENCE FOR A CHROMATOGRAPHIC CHIRAL RECOGNITION RATIONALE
UCCELLOBARRETTA, G
ROSINI, C
PINI, D
SALVADORI, P
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1990, 112 (07) : 2707 - 2710
[4] EFFECTS OF LONG-TERM ADMINISTRATION OF (4S)-1-METHYL-3-((2S)-2-[N-((1S)-1-ETHOXYCARBONYL-3-PHENYLPROPYL)AMINO]PROPIONYL)-2-OXOIMIDAZOLIDINE-4-CARBOXYLIC ACID HYDROCHLORIDE (TA-6366), A NEW ANGIOTENSIN-I CONVERTING ENZYME (ACE) INHIBITOR, FROM THE PRE-HYPERTENSIVE STAGE ON MORPHOLOGICAL CHANGE AND MECHANICAL PROPERTY RELATED TO SODIUM-ION PERMEABILITY IN AORTA OF SPONTANEOUSLY HYPERTENSIVE RATS (SHRS)
KUBO, M
KOBAYASHI, K
ISHIDA, R
JOURNAL OF PHARMACOBIO-DYNAMICS, 1992, 15 (11): : 657 - 665

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