STRUCTURAL-ANALYSIS OF OLIGOSACCHARIDE CHAINS OF GLYCOLIPIDS BY 2-DIMENSIONAL NMR

被引：6
|
作者：
INAGAKI, F
机构：
[1] Department of Molecular Physiology, Tokyo Metropolitan Institute of Medical Science, Tokyo, 113, 3–18–22, Honkomagome, Bunkyo-ku
来源：
MAGNETIC RESONANCE IN CHEMISTRY | 1992年 / 30卷
关键词：
H-1; NMR; GLYCOLIPIDS; COSY; RELAYED COSY; DOUBLE-RELAYED COSY; HOMONUCLEAR HARTMANN-HAHN (HOHAHA); RELAYED HOHAHA; NOESY;
D O I：
10.1002/mrc.1260301321
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Coherence transfer methods, such as multiple-relayed COSY and homonuclear Hartmann-Hahn spectroscopy, were applied to extract subspectra of constituent monosaccharides, which allowed complete assignments of the proton resonances of oligosaccharide chains of glycolipids. The chemical structure of oligosaccharide chains of glycolipids could be determined by the combination of coherence transfer methods and NOESY experiments.
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页码：S125 / S133
页数：9
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