Synthesis and Structure Elucidation of N '-(4-Methoxybenzylidene)-5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide

被引：3

作者：

Alotaibi, Mohammad Hayal ^{[1
]}

Mohamed, Hanan A. ^{[2
,3
]}

Abdel-Wahab, Bakr F. ^{[2
,3
]}

Hegazy, Amany S. ^{[4
]}

Kariuki, Benson M. ^{[4
]}

El-Hiti, Gamal A. ^{[5
]}

机构：

[1] King Abdulaziz City Sci & Technol, Natl Ctr Petrochem Technol, POB 6086, Riyadh 11442, Saudi Arabia

[2] Shaqra Univ, Dept Chem, Coll Sci & Humanities, POB 33, Duwadimi 11911, Saudi Arabia

[3] Natl Res Ctr, Appl Organ Chem Dept, Giza 12622, Egypt

[4] Cardiff Univ, Sch Chem, Main Bldg,Pk Pl, Cardiff CF10 3AT, Wales

[5] King Saud Univ, Dept Optometry, Coll Appl Med Sci, POB 10219, Riyadh 11433, Saudi Arabia

来源：

MOLBANK | 2018年 / 04期

关键词：

1,2,3-triazoles; carbohydrazides; single crystal X-ray diffraction; spectroscopic structural analysis; heterocycles;

D O I：

10.3390/M1034

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

N'-(4-Methoxybenzylidene)-5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide (3) was synthesized in a yield of 88% from an acid-catalyzed reaction of 5-methyl-1-phenyl-1H-1,2,3-triazole-4-carbohydrazide and 4-methoxybenzaldehyde in ethanol under reflux for 2.5 h. The structure of 3 was confirmed by the data obtained from infrared, nuclear magnetic resonance, mass spectroscopy, single crystal X-ray diffraction, and microanalysis.

引用

页数：5

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