2-[1-(2-Hydroxy-4-methoxyphenyl)ethylidene]-N-methylhydrazinecarbothioamide

被引：3

作者：

Anderson, Brian J. ^{[1
]}

Freedman, Michael B. ^{[1
]}

Millikan, Sean P. ^{[1
]}

Jasinski, Jerry P. ^{[1
]}

机构：

[1] Keene State Coll, Dept Chem, 229 Main St, Keene, NH 03435 USA

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷

基金：

美国国家科学基金会;

关键词：

data-to-parameter ratio = 26.0; meanω(C - C) = 0.004 A °; Rfactor = 0.076; single-crystal X-ray study; T = 173 K; wRfactor = 0.231;

D O I：

10.1107/S1600536813019831

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C11H15N3O2S, the dihedral angle between the mean planes of the benzene ring and hydrazinecarbothioamide group is 9.2 (1)degrees. An intramolecular O-H center dot center dot center dot N hydrogen bond is observed, serving to maintain an approximately planar conformation for the molecule. In the crystal, inversion dimers linked by C-H center dot center dot center dot O interactions occur. Further C-H center dot center dot center dot O contacts link dimers into (010) chains.

引用

页码：O1315 / +

页数：8

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