A SIMPLE AND HIGHLY DIASTEREOSELECTIVE PREPARATION OF GLYCAL EPOXIDES USING THE MCPBA-KF COMPLEX

被引：45

作者：

BELLUCCI, G ^{[1
]}

CATELANI, G ^{[1
]}

CHIAPPE, C ^{[1
]}

DANDREA, F ^{[1
]}

机构：

[1] UNIV PISA,DIPARTIMENTO CHIM BIOORGAN,I-56126 PISA,ITALY

来源：

TETRAHEDRON LETTERS | 1994年 / 35卷 / 45期

关键词：

D O I：

10.1016/S0040-4039(00)74426-1

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Glycols ore converted to the corresponding epoxides in high yields by a diastereoselective one-step epoxidation using the m-chloroperoxybenzoic acid-KF complex in anhydrous dichloromethane.

引用

页码：8433 / 8436

页数：4

共 19 条

[1] A NEW SYNTHESIS OF L-ASCORBIC-ACID FROM D-GALACTOSE
BARILI, PL
BERTI, G
DANDREA, F
DIBUSSOLO, V
GRANUCCI, I
[J]. TETRAHEDRON, 1992, 48 (30) : 6273 - 6284
[2] BARILI PL, 1992, GAZZ CHIM ITAL, V122, P135
[3] BARILI PL, 1994, 22 C NAZ DIV CHIM OR
[4] BELLUCCI G, 1994, 5 C NAZ CHIM CARB RO, P42
[5] BRIGL P, 1921, Z PHYSIOL CHEM, V116, P1
[6] BRIGL PZ, 1922, Z PHYSL CHEM, V122, P245
[7] META-CHLOROPEROXYBENZOIC ACID POTASSIUM FLUORIDE SYSTEM - STUDY OF ITS STABILITY AND REACTION WITH ALPHA-METHYLSTYRENE
CAMPS, F
COLL, J
MESSEGUER, A
PUJOL, F
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1982, 47 (27) : 5402 - 5404
[8] EBY R, 1982, CARBOHYD RES, V102, P1, DOI 10.1016/S0008-6215(00)88045-3
[9] RITTER-LIKE REACTIONS OF 1,2-ANHYDROPYRANOSE DERIVATIVES
GORDON, DM
DANISHEFSKY, SJ
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1991, 56 (11) : 3713 - 3715
[10] GUTHRIE RD, 1972, CARBOHYDRATES A, V1, P423

← 1 2 →