Chlorido{N-[(diethylamino)dimethyl-silyl]anilido-kappa N}(N,N,N',N'-tetramethyl-ethane-1,2-diamine-kappa N-2,N')iron(II)

被引：0
作者：
Chen, Juan [1 ]
机构：
[1] Taiyuan Teachers Coll, Dept Chem, Taiyuan 030031, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
data-to-parameter ratio = 18.7; mean ω(C-C) = 0.010 Å; R factor = 0.060; single-crystal X-ray study; T = 293 K; wR factor = 0.190;
D O I：
10.1107/S1600536812044741
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title iron(II) complex, [Fe(C12H21N2Si)Cl(C6H16N2)], the Fe II cation is coordinated by two N atoms from the tetramethylethane-1,2-diamine ligand [Fe-N = 2.191 (5) and 2.215 (4) angstrom], one N atom from the N-[(diethylamino)-dimethylsilyl] anilide ligand [Fe-N = 1.943 (4) angstrom] and a chloride ligand [Fe-Cl = 2.2798 (16) angstrom] in a distorted tetrahedral geometry. The N-Si-N angle is 113.9 (3)degrees. The crystal packing exhibits no short intermolecular contacts.
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收藏
页码：M1444 / +
页数：8
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