A CELL FOR EXTENDED X-RAY ABSORPTION FINE-STRUCTURE STUDIES OF OXYGEN SENSITIVE PRODUCTS OF REDOX REACTIONS

被引：15
作者：
FURENLID, LR
RENNER, MW
FAJER, J
机构：
来源：
REVIEW OF SCIENTIFIC INSTRUMENTS | 1990年 / 61卷 / 04期
关键词：
D O I：
10.1063/1.1141181
中图分类号：
TH7 [仪器、仪表];
学科分类号：
0804 ; 080401 ; 081102 ;
摘要：
We describe a cell suitable for extended x-ray absorption fine structure (EXAFS) studies of oxygen and/or water sensitive products of redox reactions. The cell utilizes aluminized Mylar windows that are transparent to x rays, provide low gas permeability, and allow vacuum to be maintained in the cell. The windows are attached to the glassware with an epoxy that resists attack by common organic solvents. Additional side arms allow multiple spectroscopic probes of the same sample under anaerobic and anhydrous conditions.
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页码：1326 / 1327
页数：2
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