DETERMINATION OF TRACES OF HAFNIUM IN ZIRCONIUM-OXIDE BY WAVELENGTH DISPERSIVE-X-RAY FLUORESCENCE SPECTROMETRY

被引:5
作者
HASANY, SM
RASHID, F
RASHID, A
REHMAN, H
机构
[1] Nuclear Chemistry Division, Pakistan Institute of Nuclear Science and Technology, Islamabad, P. O. Nilore
来源
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY-ARTICLES | 1990年 / 142卷 / 02期
关键词
D O I
10.1007/BF02040321
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An accurate and precise wavelength dispersive X-ray fluorescence spectrometric method is described for the quantitative analysis of hafnium impurities in zirconium oxide matrix in the range from 6.8 to 1004 μg/g, using the HfLβ1 line on 8420+ XRF Quantometer (ARL) with LiF (220) crystal and scintillation detector. The practical limit of measurement is 6.8 μg/g. The precision is between 1 to 6% for higher and lower concentrations of hafnium, whereas accuracy in most cases is <5%. © 1990 Akadémiai Kiadó.
引用
收藏
页码:505 / 514
页数:10
相关论文
共 10 条
  • [1] [Anonymous], 1970, ANAL CHEM ZIRCONIUM
  • [2] Elinson S.V., 1965, ANAL CHEM ZIRCONIUM
  • [3] HURTEAU MT, 1984, AECL8255 CHALK RIV N
  • [4] IHA C, 1985, INISBR268 COM NAC EN
  • [5] NAKAMURA Y, 1982, BUNSEKI KAGAKU, V31, P413
  • [6] QUANTITATIVE-DETERMINATION OF HAFNIUM IN MIXTURES OF ZIRCONIUM HAFNIUM HEXACHLORO ALKALI COMPOUNDS BY NEUTRON-ACTIVATION ANALYSIS AND X-RAY-FLUORESCENCE
    PICKLES, CA
    KIPOUROS, GJ
    FLENGAS, SN
    HANCOCK, RGV
    [J]. CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1983, 61 (09): : 2189 - 2191
  • [7] SATO IM, 1984, INISBR308 I PESQ EN
  • [8] SATO IM, 1985, IPENPUB78 I PESQ EN
  • [9] DETERMINATION OF HAFNIUM IN ZIRCONIUM AND ITS ALLOYS BY STABLE ISOTOPE-DILUTION NEUTRON-ACTIVATION ANALYSIS
    YONEZAWA, C
    KOMORI, T
    [J]. ANALYTICAL CHEMISTRY, 1983, 55 (13) : 2059 - 2062
  • [10] 1985, MULTIVARIABLE REGRES