PYROLYTIC SULFURIZATION GAS-CHROMATOGRAPHY .3. SIMULTANEOUS DETERMINATION OF ATOMIC RATIO BETWEEN C, H, O, AND N IN A METALLO-ORGANIC COMPOUND

被引:16
|
作者
HARA, T
FUJINAGA, K
TSUJI, K
机构
[1] Department of Applied Chemistry, Faculty of Engineering, Doshisha University, Karasuma Imadegawa, Kamigyo-ku, Kyoto
关键词
Compendex;
D O I
10.1246/bcsj.51.2951
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Simultaneous determination of the atomic ratio between C, H, O, and N in a metallo-organic compound containing transition element is possible by the pyrolytic sulfurization gas chromatographic method, addition of reducing agent being unnecessary. Analytical results of metallo-organic compounds depend on the characteristics of their metal oxides. A few organophosphorus compounds were analyzed. The formation of water could be predicted from the atomic ratio of carbon to oxygen in a compound.
引用
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页码:2951 / 2956
页数:6
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