SYNTHESIS AND STRUCTURAL STUDY OF NEW SILICON COMPOUND - DI-2,2'-BIPYRIDINE SILICON

被引：18

作者：

MORANCHO, R ^{[1
]}

POUVREAU, P ^{[1
]}

CONSTANT, G ^{[1
]}

JAUD, J ^{[1
]}

GALY, J ^{[1
]}

机构：

[1] LAB CHIM COORDINAT,SERV CRISTALLOG,F-31030 TOULOUSE,FRANCE

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1979年 / 166卷 / 03期

关键词：

D O I：

10.1016/S0022-328X(00)82551-6

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Low pressure sublimation of tri-2,2′-bipyridinesilicon(0) leads to di-2,2′-bipyridinesilicon crystals. The unit cell is orthorhombic, space group Pbca, a 21.509, b 15.995, c 10.127 », Z = 8. The crystal structure was solved using 490 reflexions recorded at room temperature and refined down to a reliability index R = 0.046. The silicon atom is surrounded tetrahedrally by the bidentate 2,2′-bipyridine ligand with a mean NSiN angle of 100° and a mean SiN bond length of 1.72 ». © 1979.

引用

页码：329 / 338

页数：10

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