Bis{(E)-3-[(2-hydroxybenzylidene)amino] propyl} ammonium chloride

被引：5

作者：

AlDamen, Murad A. ^{[1
]}

Haddad, Salim F. ^{[1
]}

机构：

[1] Univ Jordan, Dept Chem, Amman 11942, Jordan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 17.1; mean ω(C-C) = 0.005 Å; R factor = 0.076; single-crystal X-ray study; T = 100 K; wR factor = 0.150;

D O I：

10.1107/S1600536812045424

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title salt, C20H26N3O2+center dot Cl-, lies across a twofold crystallographic axis with the central N atom of the cation and the chloride anion sitting on this axis, Z' = 0.5. There is an intramolecular hydrogen bond between the hydroxy H atom and the imino N atom. The chloride anion and the cation are connected into chains along the a axis by an N-H center dot center dot center dot Cl hydrogen bond. In the crystal, the chains are linked via CH center dot center dot center dot Cl interactions forming two-dimensional networks lying parallel to (101).

引用

收藏

页码：O3314 / +

页数：6

相关论文

共 10 条

[1] The first Mn-Zn heterometallic dinuclear compound based on Schiff base ligand N, N′-bis(salicylidene)-1,3-diaminopropane [J].

Chen, Yue-Nan ;

Ge, Ying-Ying ;

Zhou, Wei ;

Ye, Liu-Fang ;

Gu, Zhi-Gang ;

Ma, Guo-Zheng ;

Li, Wei-Shan ;

Li, Hong ;

Cai, Yue-Peng .

INORGANIC CHEMISTRY COMMUNICATIONS, 2011, 14 (08) :1228-1232

[2] Synthesis, antibacterial activities and molecular docking studies of peptide and Schiff bases as targeted antibiotics [J].

Cheng, Kui ;

Zheng, Qing-Zhong ;

Qian, Yong ;

Shi, Lei ;

Zhao, Jing ;

Zhu, Hai-Liang .

BIOORGANIC & MEDICINAL CHEMISTRY, 2009, 17 (23) :7861-7871

[3] THE ANALYTICAL CALCULATION OF ABSORPTION IN MULTIFACETED CRYSTALS [J].

CLARK, RC ;

REID, JS .

ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :887-897

[4] OLEX2: a complete structure solution, refinement and analysis program [J].

Dolomanov, Oleg V. ;

Bourhis, Luc J. ;

Gildea, Richard J. ;

Howard, Judith A. K. ;

Puschmann, Horst .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2009, 42 :339-341

[5]

Oxford Diffraction, 2009, CRYSALIS PRO

[6]

Pavel K., 2007, POLYHEDRON, V26, P535

[7] Crystal structure of N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine [J].

Ramazania, A. ;

Dolatyari, L. ;

Morsali, A. ;

Yilmaz, V. T. ;

Bueyuekguengoer, O. .

JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2006, 3 (04) :367-370

[8] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[9] Syntheses, characterization, biological activities and photophysical properties of lanthanides complexes with a tetradentate Schiff base ligand [J].

Taha, Ziyad A. ;

Ajlouni, Abdulaziz M. ;

Al Momani, Waleed ;

Al-Ghzawi, Abeer A. .

SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2011, 81 (01) :570-577

[10] Syntheses, characterization, biological activity and fluorescence properties of bis-(salicylaldehyde)-1,3-propylenediimine Schiff base ligand and its lanthanide complexes [J].

Taha, Ziyad A. ;

Ajlouni, Abdulaziz M. ;

Al-Hassan, Khader A. ;

Hijazi, Ahmed K. ;

Faiq, Ari B. .

SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2011, 81 (01) :317-323