SIMPLE METHOD FOR MICROGRAM AMOUNTS OF SULFATE IN ATMOSPHERIC PARTICULATES

被引:12
作者
HOFFER, EM [1 ]
KOTHNY, EL [1 ]
APPEL, BR [1 ]
机构
[1] CALIF STATE DEPT HLTH,LAB SERV BRANCH,AIR & IND HYG LAB,BERKELEY,CA 94704
关键词
D O I
10.1016/0004-6981(79)90173-2
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
A simple, manual procedure is described which is useful for the analysis of water-soluble sulfate in low volume ( = 20m3) filter samples. The technique uses an aqueous extraction and an exchange reaction between a barium-nitrosulfonazo III chelate and sulfate in aqueous acetonitrile. Decrease of absorbance at 642 nm is measured in a double beam spectrophotometer. The method has been evaluated for extraction efficiency, precision, accuracy, working range, equivalence to other methods, and interferences. © 1979.
引用
收藏
页码:303 / 306
页数:4
相关论文
共 23 条
[1]   IMPROVED TITRATION MEDIUM FOR SULPHATE-ION INDICATORS [J].
ARCHER, EE ;
WHITE, DC ;
MACKISON, R .
ANALYST, 1971, 96 (1149) :879-&
[2]  
Bertolacini R. J., 1957, ANAL CHEM, V29, P281, DOI [10.1021/ac60122a031ANCHAM0003-2700, DOI 10.1021/AC60122A031ANCHAM0003-2700]
[3]   ULTRAVIOLET SPECTROPHOTOMETRIC DETERMINATION OF SULFATE, CHLORIDE, AND FLUORIDE WITH CHLORANILIC ACID [J].
BERTOLACINI, RJ ;
BARNEY, JE .
ANALYTICAL CHEMISTRY, 1958, 30 (02) :202-205
[4]   NATURE AND POSSIBLE ORIGIN OF ACID PARTICLES OBSERVED AT SWEDISH WEST COAST [J].
BROSSET, C ;
ANDREASSON, K ;
FERM, M .
ATMOSPHERIC ENVIRONMENT, 1975, 9 (6-7) :631-642
[5]   DETERMINATION OF SULPHUR AND SULPHATE BY TITRATION WITH BARIUM PERCHLORATE - COMPARISON OF VARIOUS COLOUR INDICATORS [J].
BUDESINSKY, B ;
KRUMLOVA, L .
ANALYTICA CHIMICA ACTA, 1967, 39 (03) :375-+
[6]   LINEARIZING CALIBRATION CURVE IN DETERMINATION OF SULFATE BY METHYLTHYMOL BLUE METHOD [J].
COLOVOS, G ;
PANESAR, MR ;
PARRY, EP .
ANALYTICAL CHEMISTRY, 1976, 48 (12) :1693-1696
[7]   AMBIENT AIR ANALYSIS WITH DICHOTOMOUS SAMPLER AND X-RAY-FLUORESCENCE SPECTROMETER [J].
DZUBAY, TG ;
STEVENS, RK .
ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1975, 9 (07) :663-668
[8]   DETERMINATION OF SULPHATE BY AUTOMATIC COLORIMETRIC ANALYSIS [J].
GALES, ME ;
KAYLOR, WH ;
LONGBOTTOM, JE .
ANALYST, 1968, 93 (1103) :97-+
[9]   CHARACTERIZATION OF AEROSOLS IN CALIFORNIA BY X-RAY-INDUCED X-RAY-FLUORESCENCE ANALYSIS [J].
GIAUQUE, RD ;
GODA, LY ;
BROWN, NE .
ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1974, 8 (05) :436-441
[10]  
HERMANCE HW, 1971, ENVIRON SCI TECHNOL, V5, P781