CINNOLINES .13. STRUCTURE AND REACTIONS OF ANHYDRO-BASE OF 4-HYDROXY-2-METHYLCINNOLINIUM HYDROXIDE

被引：22

作者：

AMES, DE

NOVITT, B

机构：

[1] Department of Chemistry, Chelsea College of Science and Technology, London S.W.3, Manresa Road

来源：

JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC | 1969年 / 18期

关键词：

D O I：

10.1039/j39690002355

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

1,3-Dipolar cycloaddition of dimethyl acetylenedicarboxylate to the anhydro-base of 4-hydroxy-2-methylcinnolinium hydroxide is described. Alkylation of the anhydro-base with triethyloxonium fluoroborate gives 4-ethoxy-2-methylcinnolinium fluoroborate and 1-methyl-4-cinnolone similarly gives 4-ethoxy-1-methyl-cinnolinium fluoroborate.

引用

页码：2355 / &

共 14 条

[1] CINNOLINES .6. TAUTOMERISM AND ALKYLATION OF 4-HYDROXYCINNOLINE
AMES, DE
CHAPMAN, RF
KUCHARSK.HZ
WAITE, D
[J]. JOURNAL OF THE CHEMICAL SOCIETY, 1965, (OCT): : 5391 - &
[2] CINNOLINES .12. 1,3-DIPHENYL-2H-PYRROLO[3,4-C]CINNOLINE . STRUCTURE AND N-ETHYL DERIVATIVES
AMES, DE
ANSARI, HR
ELLIS, AW
[J]. JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1969, (13): : 1795 - &
[3] CINNOLINES .8. METHYLATION OF SOME SUBSTITUTED CINNOLINES
AMES, DE
CHAPMAN, RF
WAITE, D
[J]. JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1966, (04): : 470 - &
[4] CINNOLINES .2. STRUCTURES OF N-METHYCINNOLONES
AMES, DE
KUCHARSKI, HZ
[J]. JOURNAL OF THE CHEMICAL SOCIETY, 1963, (OCT): : 4924 - &
[5] AMES DE, 1964, J CHEM SOC, P5659
[6] A NEW CINNOLINE SYNTHESIS .2. SYNTHESIS OF 1-SUBSTITUTED 4-CINNOLONE-3-CARBOXYLIC ACIDS
BARBER, HJ
LUNT, E
[J]. JOURNAL OF THE CHEMICAL SOCIETY, 1965, (FEB): : 1468 - &
[7] THE INFRARED SPECTRA OF SOME ESTERS, NITRILES, AND ESTER-NITRILES
FELTON, DGI
ORR, SFD
[J]. JOURNAL OF THE CHEMICAL SOCIETY, 1955, : 2170 - 2176
[8] 1.3-DIPOLARE CYCLOADDITIONEN - RUCKSCHAU UND AUSBLICK
HUISGEN, R
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1963, 75 (13) : 604 - +
[9] Huisgen R., 1967, ANGEW CHEM, V79, P320
[10] KATO H, 1967, TETRAHEDRON LETT, P4261

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