A USEFUL SYNTHESIS OF CHIRAL SULFONYL CYANIDES - (1S,2S,5R)-2-ISOPROPYL-5-METHYLCYCLOHEXANESULFONYL CYANIDE

被引：25

作者：

BLANCO, JM ^{[1
]}

CAAMANO, O ^{[1
]}

FERNANDEZ, F ^{[1
]}

GOMEZ, G ^{[1
]}

LOPEZ, C ^{[1
]}

机构：

[1] UNIV SANTIAGO,FAC FARM,DEPT QUIM ORGAN,E-15706 SANTIAGO,SPAIN

来源：

TETRAHEDRON-ASYMMETRY | 1992年 / 3卷 / 06期

关键词：

D O I：

10.1016/S0957-4166(00)80515-7

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A convenient method for the preparation of chiral alkanesulfonyl cyanides, by oxidation of readily available alkyl thiocyanates with m-ClC6H4CO3H, has been developed.

引用

页码：749 / 752

页数：4

共 14 条

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[2] SYNTHESIS OF SULFINYL CYANIDES
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MEYER, H
WILDEMAN, J
VANLEUSEN, AM
[J]. SYNTHETIC COMMUNICATIONS, 1975, 5 (02) : 147 - 154
[3] CAAMANO O, 1988, HETEROCYCLES, V27, P2839
[4] SYNTHESIS OF CARBOCYCLIC AMINONUCLEOSIDES
DALUGE, S
VINCE, R
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1978, 43 (12) : 2311 - 2320
[5] DIELS-ALDER CYCLOADDITIONS OF SULFONYL CYANIDES WITH CYCLOPENTADIENE - SYNTHESIS OF "2-AZABICYCLO[2.2.1]HEPTA-2,5-DIENES
JAGT, JC
VANLEUSE.AM
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1974, 39 (04) : 564 - 566
[6] JAGT JC, 1973, RECL TRAV CHIM PAY B, V92, P1343
[7] JAGT JC, 1975, RECL TRAV CHIM PAY B, V94, P12
[8] KINETIC CYANATIONS OF KETONE ENOLATES
KAHNE, D
COLLUM, DB
[J]. TETRAHEDRON LETTERS, 1981, 22 (50) : 5011 - 5014
[9] MIKOLAJCZYK M, 1987, SYNTHESIS-STUTTGART, P1009
[10] PEWS RG, 1969, J CHEM SOC CHEM COMM, P1187

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